(S)-tert-butyl 1-((5-methylfuran-2-yl)methylamino)-1-oxo-3-phenylpropan-2-ylcarbamate

Base Information

Chemical Name:(S)-tert-butyl 1-((5-methylfuran-2-yl)methylamino)-1-oxo-3-phenylpropan-2-ylcarbamate
CAS No.:1429229-34-4
Molecular Formula:C₂₀H₂₆N₂O₄
Molecular Weight:358.437
Hs Code.:

Synonyms:(S)-tert-butyl 1-((5-methylfuran-2-yl)methylamino)-1-oxo-3-phenylpropan-2-ylcarbamate

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Chemical Property of (S)-tert-butyl 1-((5-methylfuran-2-yl)methylamino)-1-oxo-3-phenylpropan-2-ylcarbamate

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Technology Process of (S)-tert-butyl 1-((5-methylfuran-2-yl)methylamino)-1-oxo-3-phenylpropan-2-ylcarbamate

There total 1 articles about (S)-tert-butyl 1-((5-methylfuran-2-yl)methylamino)-1-oxo-3-phenylpropan-2-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 14003-16-8
5-methylfurfurylamine

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 1429229-34-4
(S)-tert-butyl 1-((5-methylfuran-2-yl)methylamino)-1-oxo-3-phenylpropan-2-ylcarbamate

Guidance literature:: With 4-methyl-morpholine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at -15 ℃; for 1h;
DOI:10.1016/j.tetlet.2013.02.067

Reference yield: 85.0%

: 1429229-34-4
(S)-tert-butyl 1-((5-methylfuran-2-yl)methylamino)-1-oxo-3-phenylpropan-2-ylcarbamate

: 1429229-19-5
(S)-4-benzyl-6-methyl-1,2-dihydropyrrolo[1,2-a]pyrazin-3(4H)-one

Guidance literature:: (S)-tert-butyl 1-((5-methylfuran-2-yl)methylamino)-1-oxo-3-phenylpropan-2-ylcarbamate; With hydrogenchloride; acetic acid; In water; at 0 - 20 ℃; for 12h;

With sodium hydrogencarbonate; In water; for 3h; pH=Ca. 7; Reflux;
DOI:10.1016/j.tetlet.2013.02.067

Reference yield:

: 1429229-34-4
(S)-tert-butyl 1-((5-methylfuran-2-yl)methylamino)-1-oxo-3-phenylpropan-2-ylcarbamate

: 1429229-30-0
(S)-4-benzyl-6-methyl-1,2,3,4-tetrahydropyrrolo[1,2-a]pyrazine

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride; acetic acid / water / 12 h / 0 - 20 °C

1.2: 3 h / pH Ca_. 7 / Reflux

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 - 70 °C

With hydrogenchloride; lithium aluminium tetrahydride; acetic acid; In tetrahydrofuran; water;
DOI:10.1016/j.tetlet.2013.02.067