(E)-methyl 2--4-(diethoxyphosphinyl)-2-butenoate

Base Information

Chemical Name:(E)-methyl 2--4-(diethoxyphosphinyl)-2-butenoate
CAS No.:133753-37-4
Molecular Formula:C₁₇H₂₄NO₇P
Molecular Weight:385.354
Hs Code.:

(E)-methyl 2-<N-(benzyloxycarbonyl)amino>-4-(diethoxyphosphinyl)-2-butenoate

Synonyms:(E)-methyl 2--4-(diethoxyphosphinyl)-2-butenoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-methyl 2--4-(diethoxyphosphinyl)-2-butenoate

Chemical Property:

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Technology Process of (E)-methyl 2--4-(diethoxyphosphinyl)-2-butenoate

There total 3 articles about (E)-methyl 2--4-(diethoxyphosphinyl)-2-butenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 133753-36-3
(Z)-methyl 2--4-(diethoxyphosphinyl)-2-butenoate

: 133753-37-4
(E)-methyl 2--4-(diethoxyphosphinyl)-2-butenoate

Guidance literature:: In acetone; at 20 ℃; for 120h; Yield given; Irradiation;
DOI:10.1021/jm00109a023

Reference yield:

: 1606-75-3
(2-oxoethyl)phosphonic acid diethyl ester

: 133753-37-4
(E)-methyl 2--4-(diethoxyphosphinyl)-2-butenoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) potassium tert-butoxide / 1.) CH₂Cl₂, -78 deg C, 20 min, 2.) CH₂Cl₂, RT, 2 h

2: acetone / 120 h / 20 °C / Irradiation

With potassium tert-butylate; In acetone;
DOI:10.1021/jm00109a023

Reference yield:

: 100945-15-1,88568-95-0
N-(benzyloxycarbonyl)phosphonoglycine trimethyl ester

: 133753-37-4
(E)-methyl 2--4-(diethoxyphosphinyl)-2-butenoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) potassium tert-butoxide / 1.) CH₂Cl₂, -78 deg C, 20 min, 2.) CH₂Cl₂, RT, 2 h

2: acetone / 120 h / 20 °C / Irradiation

With potassium tert-butylate; In acetone;
DOI:10.1021/jm00109a023