1-(1,4-dihydro-5,8-dimethoxy-1,4-dioxonaphthalen-6-yl)-4-methylpent-3-enyl 2-(4-methoxyphenyl)acetate

Base Information

Chemical Name:1-(1,4-dihydro-5,8-dimethoxy-1,4-dioxonaphthalen-6-yl)-4-methylpent-3-enyl 2-(4-methoxyphenyl)acetate
CAS No.:1314765-86-0
Molecular Formula:C₂₇H₂₈O₇
Molecular Weight:464.515
Hs Code.:

Synonyms:1-(1,4-dihydro-5,8-dimethoxy-1,4-dioxonaphthalen-6-yl)-4-methylpent-3-enyl 2-(4-methoxyphenyl)acetate

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Chemical Property of 1-(1,4-dihydro-5,8-dimethoxy-1,4-dioxonaphthalen-6-yl)-4-methylpent-3-enyl 2-(4-methoxyphenyl)acetate

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Technology Process of 1-(1,4-dihydro-5,8-dimethoxy-1,4-dioxonaphthalen-6-yl)-4-methylpent-3-enyl 2-(4-methoxyphenyl)acetate

There total 4 articles about 1-(1,4-dihydro-5,8-dimethoxy-1,4-dioxonaphthalen-6-yl)-4-methylpent-3-enyl 2-(4-methoxyphenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.4%

: 104-01-8
4-Methoxyphenylacetic acid

: 1031235-90-1
(R)-6-(1-hydroxy-4-methylpent-3-enyl)-5,8-dimethoxynaphthalene-1,4-dione

: 1314765-86-0
1-(1,4-dihydro-5,8-dimethoxy-1,4-dioxonaphthalen-6-yl)-4-methylpent-3-enyl 2-(4-methoxyphenyl)acetate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.ejmech.2011.05.006

Reference yield:

: 1031235-88-7
1-[1,4-dimethoxy-5,8-bis-(methoxymethoxy)-naphthalen-2-yl]-4-methylpent-3-en-1-ol

: 1314765-86-0
1-(1,4-dihydro-5,8-dimethoxy-1,4-dioxonaphthalen-6-yl)-4-methylpent-3-enyl 2-(4-methoxyphenyl)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / tetrahydrofuran; water; isopropyl alcohol / 3 h / 20 °C

2: dmap; dicyclohexyl-carbodiimide / dichloromethane / 20 °C / Inert atmosphere

With hydrogenchloride; dmap; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; water; isopropyl alcohol;
DOI:10.1016/j.ejmech.2011.05.006

Reference yield:

: 1253934-34-7
2-(1-hydroxy-4-methylpent-3-enyl)-5,8-bis-(methoxymethoxy)-naphthalene-1,4-dione

: 1314765-86-0
1-(1,4-dihydro-5,8-dimethoxy-1,4-dioxonaphthalen-6-yl)-4-methylpent-3-enyl 2-(4-methoxyphenyl)acetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium dithionite / tetrahydrofuran; water / 20 °C / Inert atmosphere

1.2: 40 °C / Inert atmosphere; Reflux

2.1: hydrogenchloride / tetrahydrofuran; water; isopropyl alcohol / 3 h / 20 °C

3.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 20 °C / Inert atmosphere

With hydrogenchloride; dmap; sodium dithionite; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; water; isopropyl alcohol;
DOI:10.1016/j.ejmech.2011.05.006