C₂₉H₂₉N₃O₆S

Base Information

Chemical Name:C₂₉H₂₉N₃O₆S
CAS No.:1616280-27-3
Molecular Formula:C₂₉H₂₉N₃O₆S
Molecular Weight:547.632
Hs Code.:

C<sub>29</sub>H<sub>29</sub>N<sub>3</sub>O<sub>6</sub>S

Synonyms:C₂₉H₂₉N₃O₆S

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Chemical Property of C₂₉H₂₉N₃O₆S

Chemical Property:

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Technology Process of C₂₉H₂₉N₃O₆S

There total 22 articles about C₂₉H₂₉N₃O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1616280-24-0
C₃₀H₃₁N₃O₆S

: 1616280-27-3
C₂₉H₂₉N₃O₆S

Guidance literature:: C₃₀H₃₁N₃O₆S; With water; lithium hydroxide; In acetonitrile; at 20 ℃;

With hydrogenchloride; In water; acetonitrile;

Reference yield:

: 918305-51-8
methyl (2E)-3-(6-bromopyridin-3-yl)prop-2-enoate

: 1616280-27-3
C₂₉H₂₉N₃O₆S

Guidance literature:: Multi-step reaction with 6 steps

1: nickel dichloride; sodium tetrahydroborate / methanol / 0.33 h / 0 °C

2: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / tetrahydrofuran / 50 °C

3: potassium carbonate / methanol; tetrahydrofuran / 1 h / 20 °C

4: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / tetrahydrofuran / 4 h / 20 - 50 °C / Inert atmosphere

5: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 55 °C

6: lithium hydroxide; water / acetonitrile / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; sodium tetrahydroborate; copper(l) iodide; tetrabutyl ammonium fluoride; water; potassium carbonate; triethylamine; nickel dichloride; lithium hydroxide; In tetrahydrofuran; methanol; acetonitrile; 2: |Sonogashira Cross-Coupling / 4: |Sonogashira Cross-Coupling;

Reference yield:

: 1616279-53-8
methyl 4-azido-4-(2-chloro-5-nitrophenyl)butanoate

: 1616280-27-3
C₂₉H₂₉N₃O₆S

Guidance literature:: Multi-step reaction with 9 steps

1.1: triphenylphosphine / N,N-dimethyl-formamide / 2 h / 90 °C

1.2: 16 h / 90 °C

2.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0.17 h / 0 °C

2.2: 1 h / 20 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 6 h / 120 °C

4.1: ammonium chloride; iron / methanol; tetrahydrofuran; water / 1 h / 100 °C

5.1: potassium iodide; potassium iodate; hydrogenchloride / methanol; water; 1,4-dioxane / 1.5 h / 50 °C / Inert atmosphere

6.1: pyridine / 0.75 h / 0 - 20 °C

7.1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / tetrahydrofuran / 4 h / 20 - 50 °C / Inert atmosphere

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 55 °C

9.1: lithium hydroxide; water / acetonitrile / 20 °C

With pyridine; hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; potassium iodate; copper(l) iodide; tetrabutyl ammonium fluoride; water; iron; sodium hydride; potassium carbonate; ammonium chloride; triethylamine; triphenylphosphine; potassium iodide; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; water; N,N-dimethyl-formamide; acetonitrile; 7.1: |Sonogashira Cross-Coupling;