2(C₆H₅)6PNP⁽¹⁺⁾*Ir⁽¹⁺⁾*CO*CN^(1-)*S₂C₂(CN)2^(2-) = [(C₆H₅)3PNP(C₆H₅)3]2[Ir(CO)(CN)(S₂C₂(CN)2)]

Base Information

• Chemical Name: 2(C₆H₅)6PNP⁽¹⁺⁾*Ir⁽¹⁺⁾*CO*CN^(1-)*S₂C₂(CN)2^(2-) = [(C₆H₅)3PNP(C₆H₅)3]2[Ir(CO)(CN)(S₂C₂(CN)2)]
• CAS No.: 84642-25-1
• Molecular Formula: CN*CO*C₄N₂S₂*2C₃₆H₃₀NP₂*Ir
• Molecular Weight: 1463.61

Synonyms:2(C₆H₅)6PNP⁽¹⁺⁾*Ir⁽¹⁺⁾*CO*CN^(1-)*S₂C₂(CN)2^(2-) = [(C₆H₅)3PNP(C₆H₅)3]2[Ir(CO)(CN)(S₂C₂(CN)2)]

Chemical Property of 2(C₆H₅)6PNP⁽¹⁺⁾*Ir⁽¹⁺⁾*CO*CN^(1-)*S₂C₂(CN)2^(2-) = [(C₆H₅)3PNP(C₆H₅)3]2[Ir(CO)(CN)(S₂C₂(CN)2)]

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Technology Process of 2(C₆H₅)6PNP⁽¹⁺⁾*Ir⁽¹⁺⁾*CO*CN^(1-)*S₂C₂(CN)2^(2-) = [(C₆H₅)3PNP(C₆H₅)3]2[Ir(CO)(CN)(S₂C₂(CN)2)]

There total 1 articles about 2(C₆H₅)6PNP⁽¹⁺⁾*Ir⁽¹⁺⁾*CO*CN^(1-)*S₂C₂(CN)2^(2-) = [(C₆H₅)3PNP(C₆H₅)3]2[Ir(CO)(CN)(S₂C₂(CN)2)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

(C6H5)3PNP(C6H5)3(1+)*Ir(CO)2(S2C2(CN)2)(1-) = (C6H5)3PNP(C6H5)3[Ir(CO)2(S2C2(CN)2)] (84623-80-3) + bis(triphenylphosphine)iminium cyanide (65300-07-4) → 2(C6H5)6PNP(1+)*Ir(1+)*CO*CN(1-)*S2C2(CN)2(2-) = [(C6H5)3PNP(C6H5)3]2[Ir(CO)(CN)(S2C2(CN)2)] (84642-25-1)

Guidance literature:

In acetonitrile; byproducts: CO; under N2; to a solution of the Ir-complex was added dropwise a solutionof PPN(CN); concentrated under vacuum; 2-propanol was added; concentrated again (vacuum); was set aside at -20°C for 1 h; collected by filtration; washed twice with 2-propanol and twice with ether; elem. anal.;

DOI:10.1021/ja00345a019

upstream raw materials:

(C₆H₅)3PNP(C₆H₅)3⁽¹⁺⁾*Ir(CO)2(S₂C₂(CN)2)^(1-) = (C₆H₅)3PNP(C₆H₅)3[Ir(CO)2(S₂C₂(CN)2)]

bis(triphenylphosphine)iminium cyanide

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