5-(2,4-dichloro-phenylamino)-2-ethyl-3-(1-propyl-butyl)-3H-imidazole-4-carboxylic acid methylamide

Base Information

Chemical Name:5-(2,4-dichloro-phenylamino)-2-ethyl-3-(1-propyl-butyl)-3H-imidazole-4-carboxylic acid methylamide
CAS No.:756481-38-6
Molecular Formula:C₂₀H₂₈Cl₂N₄O
Molecular Weight:411.375
Hs Code.:

5-(2,4-dichloro-phenylamino)-2-ethyl-3-(1-propyl-butyl)-3<i>H</i>-imidazole-4-carboxylic acid methylamide

Synonyms:5-(2,4-dichloro-phenylamino)-2-ethyl-3-(1-propyl-butyl)-3H-imidazole-4-carboxylic acid methylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(2,4-dichloro-phenylamino)-2-ethyl-3-(1-propyl-butyl)-3H-imidazole-4-carboxylic acid methylamide

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Technology Process of 5-(2,4-dichloro-phenylamino)-2-ethyl-3-(1-propyl-butyl)-3H-imidazole-4-carboxylic acid methylamide

There total 8 articles about 5-(2,4-dichloro-phenylamino)-2-ethyl-3-(1-propyl-butyl)-3H-imidazole-4-carboxylic acid methylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 532982-99-3
3-(2,4-dichlorophenyl)-8-ethyl-7-(4-heptyl)-1-methyl-3,7-dihydro-1H-purine-2,6-dione

: 756481-38-6
5-(2,4-dichloro-phenylamino)-2-ethyl-3-(1-propyl-butyl)-3H-imidazole-4-carboxylic acid methylamide

Guidance literature:: With sodium hydroxide; In 1,4-dioxane; ethanol; Heating;
DOI:10.1021/jm049787k

Reference yield:

: 67764-22-1
4-heptylmethane sulphonate

: 756481-38-6
5-(2,4-dichloro-phenylamino)-2-ethyl-3-(1-propyl-butyl)-3H-imidazole-4-carboxylic acid methylamide

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / dimethylformamide / 80 °C

2: aq. NaOH / dioxane; ethanol / Heating

With sodium hydroxide; potassium carbonate; In 1,4-dioxane; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm049787k

Reference yield:

: 2612-57-9
2,4-dichlorophenyl isocyanate

: 756481-38-6
5-(2,4-dichloro-phenylamino)-2-ethyl-3-(1-propyl-butyl)-3H-imidazole-4-carboxylic acid methylamide

Guidance literature:: Multi-step reaction with 7 steps

1.1: 74 percent / ethanol; tetrahydrofuran / 0.33 h / 65 °C

2.1: acetic anhydride / 3.75 h / 85 °C

2.2: 54 percent / aq. NaOH / 1 h / 60 °C

3.1: aq. NaNO₂; acetic acid / 5 h / 50 - 75 °C

4.1: aq. NH₄OH; Na₂S₂O₄ / 2.5 h / 50 °C

5.1: 85 percent / ethanol / 6 h / Heating

6.1: K₂CO₃ / dimethylformamide / 80 °C

7.1: aq. NaOH / dioxane; ethanol / Heating

With ammonium hydroxide; sodium hydroxide; sodium dithionite; acetic anhydride; potassium carbonate; acetic acid; sodium nitrite; In tetrahydrofuran; 1,4-dioxane; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm049787k