5,8-Bis-(toluene-4-sulfonyl)-1,5,8,12-tetraaza-bicyclo[10.2.2]hexadecane

Base Information

Chemical Name:5,8-Bis-(toluene-4-sulfonyl)-1,5,8,12-tetraaza-bicyclo[10.2.2]hexadecane
CAS No.:78707-09-2
Molecular Formula:C₂₆H₃₈N₄O₄S₂
Molecular Weight:534.744
Hs Code.:

Synonyms:5,8-Bis-(toluene-4-sulfonyl)-1,5,8,12-tetraaza-bicyclo[10.2.2]hexadecane

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Chemical Property of 5,8-Bis-(toluene-4-sulfonyl)-1,5,8,12-tetraaza-bicyclo[10.2.2]hexadecane

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Technology Process of 5,8-Bis-(toluene-4-sulfonyl)-1,5,8,12-tetraaza-bicyclo[10.2.2]hexadecane

There total 3 articles about 5,8-Bis-(toluene-4-sulfonyl)-1,5,8,12-tetraaza-bicyclo[10.2.2]hexadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 72952-82-0
1,5,8,12-tetraazabicyclo<10.2.2>hexadecane

: 98-59-9
p-toluenesulfonyl chloride

: 78707-09-2
5,8-Bis-(toluene-4-sulfonyl)-1,5,8,12-tetraaza-bicyclo[10.2.2]hexadecane

Guidance literature:: With triethylamine; In dichloromethane; at 25 ℃; for 2h;
DOI:10.1021/ja00404a035

Reference yield:

: 295-37-4
1,4,8,11-Tetraazacyclotetradecane

: 78707-09-2
5,8-Bis-(toluene-4-sulfonyl)-1,5,8,12-tetraaza-bicyclo[10.2.2]hexadecane

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / methanol / 0.5 h / 0 °C

2: 96 percent / diisobutylaluminum hydride / 1.) n-hexane, 0-25 deg C, 2.) toluene, reflux, 4 d

3: 72 percent / triethylamine / CH₂Cl₂ / 2 h / 25 °C

With diisobutylaluminium hydride; triethylamine; In methanol; dichloromethane;
DOI:10.1021/ja00404a035

Reference yield:

: 72738-47-7
decahydro-1H,6H-3a,5a,8a,10a-tetraazapyrene

: 78707-09-2
5,8-Bis-(toluene-4-sulfonyl)-1,5,8,12-tetraaza-bicyclo[10.2.2]hexadecane

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / diisobutylaluminum hydride / 1.) n-hexane, 0-25 deg C, 2.) toluene, reflux, 4 d

2: 72 percent / triethylamine / CH₂Cl₂ / 2 h / 25 °C

With diisobutylaluminium hydride; triethylamine; In dichloromethane;
DOI:10.1021/ja00404a035