6-(benzyloxy)-N-(4-tert-butylbenzyl)-2-methyl-1,8-naphthyridine-3-carboxamide

Base Information

Chemical Name:6-(benzyloxy)-N-(4-tert-butylbenzyl)-2-methyl-1,8-naphthyridine-3-carboxamide
CAS No.:1241911-49-8
Molecular Formula:C₂₈H₂₉N₃O₂
Molecular Weight:439.557
Hs Code.:

Synonyms:6-(benzyloxy)-N-(4-tert-butylbenzyl)-2-methyl-1,8-naphthyridine-3-carboxamide

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Chemical Property of 6-(benzyloxy)-N-(4-tert-butylbenzyl)-2-methyl-1,8-naphthyridine-3-carboxamide

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Technology Process of 6-(benzyloxy)-N-(4-tert-butylbenzyl)-2-methyl-1,8-naphthyridine-3-carboxamide

There total 5 articles about 6-(benzyloxy)-N-(4-tert-butylbenzyl)-2-methyl-1,8-naphthyridine-3-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 1241910-53-1
N-(4-tert-butylbenzyl)-6-iodo-2-methyl-1,8-naphthyridine-3-carboxamide

: 100-51-6,185532-71-2
benzyl alcohol

: 1241911-49-8
6-(benzyloxy)-N-(4-tert-butylbenzyl)-2-methyl-1,8-naphthyridine-3-carboxamide

Guidance literature:: With caesium carbonate; copper(l) iodide; 3,4,7,8-Tetramethyl-o-phenanthrolin; at 120 ℃; Inert atmosphere; sealed tube;

Reference yield:

: 7521-41-7
2-Aminonicotinaldehyde

: 1241911-49-8
6-(benzyloxy)-N-(4-tert-butylbenzyl)-2-methyl-1,8-naphthyridine-3-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: iodine; sulfuric acid; acetic acid; periodic acid / water / 4 h / 80 °C

2: piperidine / 2 h / 120 °C / Sealed pressure tube

3: caesium carbonate; copper(l) iodide; 3,4,7,8-Tetramethyl-o-phenanthrolin / 120 °C / Sealed pressure tube; Inert atmosphere

With piperidine; copper(l) iodide; 3,4,7,8-Tetramethyl-o-phenanthrolin; sulfuric acid; iodine; caesium carbonate; acetic acid; periodic acid; In water;

Reference yield:

: 39895-55-1
4-(1,1-dimethylethyl)-benzenemethanamine

: 1241911-49-8
6-(benzyloxy)-N-(4-tert-butylbenzyl)-2-methyl-1,8-naphthyridine-3-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / 28 h / 130 °C

2: piperidine / 2 h / 120 °C / Sealed pressure tube

3: caesium carbonate; copper(l) iodide; 3,4,7,8-Tetramethyl-o-phenanthrolin / 120 °C / Sealed pressure tube; Inert atmosphere

With piperidine; copper(l) iodide; 3,4,7,8-Tetramethyl-o-phenanthrolin; caesium carbonate; In toluene;