H₂N₈C₃₂H₉(OC₆H₄C(CH₃)3)6C₆H₄CH₂N₃

Base Information

• Chemical Name: H₂N₈C₃₂H₉(OC₆H₄C(CH₃)3)6C₆H₄CH₂N₃
• CAS No.: 1048951-00-3
• Molecular Formula: C₉₉H₉₅N₁₁O₆
• Molecular Weight: 1534.91
• Mol file: 1048951-00-3.mol

Synonyms:H₂N₈C₃₂H₉(OC₆H₄C(CH₃)3)6C₆H₄CH₂N₃

Chemical Property of H₂N₈C₃₂H₉(OC₆H₄C(CH₃)3)6C₆H₄CH₂N₃

Chemical Property:

Purity/Quality:

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Technology Process of H₂N₈C₃₂H₉(OC₆H₄C(CH₃)3)6C₆H₄CH₂N₃

There total 1 articles about H₂N₈C₃₂H₉(OC₆H₄C(CH₃)3)6C₆H₄CH₂N₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

C99H95BrN8O6 (1048950-98-6) → C99H95N11O6 (1048951-00-3)

Guidance literature:

With sodium azide; In tetrahydrofuran; water; at 70 ℃; for 4h;

DOI:10.1021/ja8033262

Reference yield: 88.0%

C99H95N11O6 (1048951-00-3) → C99H93N11O6(2-)*Zn(2+) (1048964-74-4)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; zinc(II) chloride; In N,N-dimethyl-formamide; chlorobenzene; at 100 ℃; for 3h;

DOI:10.1021/ja8033262

Reference yield: 88.0%

H2N8C32H9(OC6H4C(CH3)3)6C6H4CH2N3 (1048951-00-3) + zinc(II) chloride (7646-85-7,24359-56-6) → Zn(N8C32H9(OC6H4C(CH3)3)6C6H4CH2N3) (1048964-74-4)

Guidance literature:

In N,N-dimethyl-formamide; chlorobenzene; 100°C, 3 h;

DOI:10.1021/ja8033262

upstream raw materials:

C₉₉H₉₅BrN₈O₆

Downstream raw materials:

Zn(N₈C₃₂H₉(OC₆H₄C(CH₃)3)6C₆H₄CH₂N₃)

C₉₉H₉₃N₁₁O₆^(2-)*Zn⁽²⁺⁾