(2(1')E,5E)-methyl 2-(2'-benzyloxyethylidene)-6,10-dimethyl-5,9-undecadienoate

Base Information

Chemical Name:(2(1')E,5E)-methyl 2-(2'-benzyloxyethylidene)-6,10-dimethyl-5,9-undecadienoate
CAS No.:74144-04-0
Molecular Formula:C₂₃H₃₂O₃
Molecular Weight:356.505
Hs Code.:

Synonyms:(2(1')E,5E)-methyl 2-(2'-benzyloxyethylidene)-6,10-dimethyl-5,9-undecadienoate

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Chemical Property of (2(1')E,5E)-methyl 2-(2'-benzyloxyethylidene)-6,10-dimethyl-5,9-undecadienoate

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Technology Process of (2(1')E,5E)-methyl 2-(2'-benzyloxyethylidene)-6,10-dimethyl-5,9-undecadienoate

There total 4 articles about (2(1')E,5E)-methyl 2-(2'-benzyloxyethylidene)-6,10-dimethyl-5,9-undecadienoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 71841-08-2
homogeraniol p-toluenesulfonate ester

: 74144-04-0
(2(1')E,5E)-methyl 2-(2'-benzyloxyethylidene)-6,10-dimethyl-5,9-undecadienoate

Guidance literature:: Multi-step reaction with 3 steps

1: 64 percent / dimethylsulfoxide / Ambient temperature

2: LDA, ZnCl₂ / tetrahydrofuran / 0.17 h / 0 °C

With zinc(II) chloride; lithium diisopropyl amide; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1021/ja00388a038

Reference yield:

: 71841-09-3
(E)-methyl 6,10-dimethyl-2-(phenylthio)-5,9-undecadienoate

: 74144-04-0
(2(1')E,5E)-methyl 2-(2'-benzyloxyethylidene)-6,10-dimethyl-5,9-undecadienoate

Guidance literature:: Multi-step reaction with 2 steps

1: LDA, ZnCl₂ / tetrahydrofuran / 0.17 h / 0 °C

With zinc(II) chloride; lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1021/ja00388a038

Reference yield:

: 60656-87-3
benzyloxyacetoaldehyde

: 74144-04-0
(2(1')E,5E)-methyl 2-(2'-benzyloxyethylidene)-6,10-dimethyl-5,9-undecadienoate

Guidance literature:: Multi-step reaction with 2 steps

1: LDA, ZnCl₂ / tetrahydrofuran / 0.17 h / 0 °C

With zinc(II) chloride; lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1021/ja00388a038