allyl 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-p-methoxybenzyl-β-D-glucopyranosyl-(1→4)-6-O-benzyl-3-O-benzyloxycarbonyl-2-N-trichloroethoxycarbonylamino-2-deoxy-α-D-glucopyranoside

Base Information

Chemical Name:allyl 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-p-methoxybenzyl-β-D-glucopyranosyl-(1→4)-6-O-benzyl-3-O-benzyloxycarbonyl-2-N-trichloroethoxycarbonylamino-2-deoxy-α-D-glucopyranoside
CAS No.:1215016-56-0
Molecular Formula:C₅₅H₅₉Cl₃N₄O₁₄
Molecular Weight:1106.45
Hs Code.:

allyl 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-p-methoxybenzyl-β-D-glucopyranosyl-(1→4)-6-O-benzyl-3-O-benzyloxycarbonyl-2-N-trichloroethoxycarbonylamino-2-deoxy-α-D-glucopyranoside

Synonyms:allyl 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-p-methoxybenzyl-β-D-glucopyranosyl-(1→4)-6-O-benzyl-3-O-benzyloxycarbonyl-2-N-trichloroethoxycarbonylamino-2-deoxy-α-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of allyl 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-p-methoxybenzyl-β-D-glucopyranosyl-(1→4)-6-O-benzyl-3-O-benzyloxycarbonyl-2-N-trichloroethoxycarbonylamino-2-deoxy-α-D-glucopyranoside

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Technology Process of allyl 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-p-methoxybenzyl-β-D-glucopyranosyl-(1→4)-6-O-benzyl-3-O-benzyloxycarbonyl-2-N-trichloroethoxycarbonylamino-2-deoxy-α-D-glucopyranoside

There total 2 articles about allyl 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-p-methoxybenzyl-β-D-glucopyranosyl-(1→4)-6-O-benzyl-3-O-benzyloxycarbonyl-2-N-trichloroethoxycarbonylamino-2-deoxy-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1215016-52-6
C₂₇H₃₀Cl₃NO₉

: 1215016-50-4
C₃₀H₃₁Cl₃N₄O₆

: 1215016-56-0
allyl 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-p-methoxybenzyl-β-D-glucopyranosyl-(1→4)-6-O-benzyl-3-O-benzyloxycarbonyl-2-N-trichloroethoxycarbonylamino-2-deoxy-α-D-glucopyranoside

Guidance literature:: With boron trifluoride diethyl etherate; In hexane; dichloromethane; at -78 ℃; stereoselective reaction;
DOI:10.1016/j.tetlet.2009.12.124

Reference yield:

: 1215016-52-6
C₂₇H₃₀Cl₃NO₉

: 1215016-50-4
C₃₀H₃₁Cl₃N₄O₆

: 1215016-56-0
allyl 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-p-methoxybenzyl-β-D-glucopyranosyl-(1→4)-6-O-benzyl-3-O-benzyloxycarbonyl-2-N-trichloroethoxycarbonylamino-2-deoxy-α-D-glucopyranoside

: 1215016-60-6
C₅₅H₅₉Cl₃N₄O₁₄

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In hexane; dichloromethane; at -78 ℃; optical yield given as %de;
DOI:10.1016/j.tetlet.2009.12.124