2,5-Anhydro-3-benzyl-6-deoxy-L-idose Dimethyl Acetal

Base Information

Chemical Name:2,5-Anhydro-3-benzyl-6-deoxy-L-idose Dimethyl Acetal
CAS No.:75378-67-5
Molecular Formula:C₁₅H₂₂O₅
Molecular Weight:282.337
Hs Code.:

Synonyms:2,5-Anhydro-3-benzyl-6-deoxy-L-idose Dimethyl Acetal

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Chemical Property of 2,5-Anhydro-3-benzyl-6-deoxy-L-idose Dimethyl Acetal

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Technology Process of 2,5-Anhydro-3-benzyl-6-deoxy-L-idose Dimethyl Acetal

There total 1 articles about 2,5-Anhydro-3-benzyl-6-deoxy-L-idose Dimethyl Acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 32445-69-5
(1S,3R,4S,5R)-4-Benzyloxy-3-dimethoxymethyl-2,6-dioxa-bicyclo[3.2.0]heptane

: 75378-67-5
2,5-Anhydro-3-benzyl-6-deoxy-L-idose Dimethyl Acetal

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 6h; Heating;
DOI:10.1021/jo01314a031

Reference yield:

: 75378-67-5
2,5-Anhydro-3-benzyl-6-deoxy-L-idose Dimethyl Acetal

: 75378-69-7
2,5-Anhydro-3,4-dibenzyl-6-deoxy-L-idonic Acid

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent Chromat_. / NaH / dimethylformamide / 2 h / Ambient temperature

2: 1.) H₃O+; 2.) Jones reagent / 1.) 4h reflux, acetone, THF, sulfuric acid; 2.) 0 deg C overnight

With jones reagent; oxonium; sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1021/jo01314a031

Reference yield:

: 75378-67-5
2,5-Anhydro-3-benzyl-6-deoxy-L-idose Dimethyl Acetal

: 75378-70-0
2,5-Anhydro-3,4-dibenzyl-6-deoxy-N,N-dimethyl-L-idonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent Chromat_. / NaH / dimethylformamide / 2 h / Ambient temperature

2: 1.) H₃O+; 2.) Jones reagent / 1.) 4h reflux, acetone, THF, sulfuric acid; 2.) 0 deg C overnight

3: 1.) (ClCO)2 / 1.) 2h, 100 deg C, toluene; 2.) 12h, room temp., toluene

With jones reagent; oxalyl dichloride; oxonium; sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1021/jo01314a031