Technology Process of C29H36O11
There total 4 articles about C29H36O11 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C23H26O9;
With
potassium hydrogencarbonate;
In
acetone;
for 2h;
bromoacetic acid tert-butyl ester;
With
tetrabutylammomium bromide;
In
acetone;
at 70 ℃;
for 48h;
DOI:10.1071/CH12013
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: triethylsilane; trifluoroacetic acid / dichloromethane / 2 h
2.1: potassium hydrogencarbonate / acetone / 2 h
2.2: 48 h / 70 °C
With
triethylsilane; potassium hydrogencarbonate; trifluoroacetic acid;
In
dichloromethane; acetone;
DOI:10.1071/CH12013
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: water; toluene-4-sulfonic acid / ethanol / 0.5 h / 50 °C
2.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 14 h / 0 °C
3.1: triethylsilane; trifluoroacetic acid / dichloromethane / 2 h
4.1: potassium hydrogencarbonate / acetone / 2 h
4.2: 48 h / 70 °C
With
triethylsilane; dmap; water; potassium hydrogencarbonate; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; trifluoroacetic acid;
In
ethanol; dichloromethane; acetone;
DOI:10.1071/CH12013