2-[4-(4-methoxyphenylamino)-2-oxo-2H-pyridin-1-yl]-N-isopentylacetamide

Base Information

Chemical Name:2-[4-(4-methoxyphenylamino)-2-oxo-2H-pyridin-1-yl]-N-isopentylacetamide
CAS No.:1624283-49-3
Molecular Formula:C₁₉H₂₅N₃O₃
Molecular Weight:343.426
Hs Code.:

Synonyms:2-[4-(4-methoxyphenylamino)-2-oxo-2H-pyridin-1-yl]-N-isopentylacetamide

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Chemical Property of 2-[4-(4-methoxyphenylamino)-2-oxo-2H-pyridin-1-yl]-N-isopentylacetamide

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Technology Process of 2-[4-(4-methoxyphenylamino)-2-oxo-2H-pyridin-1-yl]-N-isopentylacetamide

There total 7 articles about 2-[4-(4-methoxyphenylamino)-2-oxo-2H-pyridin-1-yl]-N-isopentylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1310383-72-2,179324-87-9
(aR,3aS,4S,6S,7aR)-hexahydro-3a,8,8-trimethyl-α-(2-methylpropyl)-4,6-methano-1,3,2-benzodioxaborole-2-methanamine 2,2,2-trifluoroacetate

: 1624283-77-7
2-[4-(4-methoxyphenylamino)-2-oxopyridin-1(2H)-yl]acetic acid

: 1624283-49-3
2-[4-(4-methoxyphenylamino)-2-oxo-2H-pyridin-1-yl]-N-isopentylacetamide

: 1624283-90-4
(R)-1-{2-[4-(4-methoxyphenylamino)-2-oxopyridin-1(2H)-yl]acetamido}-3-methylbutylboronic acid pinanediol ester

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at -15 - 20 ℃; for 3h;
DOI:10.1002/cmdc.201402075

Reference yield:

: 1310383-72-2,179324-87-9
(aR,3aS,4S,6S,7aR)-hexahydro-3a,8,8-trimethyl-α-(2-methylpropyl)-4,6-methano-1,3,2-benzodioxaborole-2-methanamine 2,2,2-trifluoroacetate

: 1624283-77-7
2-[4-(4-methoxyphenylamino)-2-oxopyridin-1(2H)-yl]acetic acid

: 1624283-49-3
2-[4-(4-methoxyphenylamino)-2-oxo-2H-pyridin-1-yl]-N-isopentylacetamide

Guidance literature:: With hydrogenchloride; Dihydroxy-isobutyl-boran; In methanol; hexane; water; at 20 ℃; for 18h;
DOI:10.1002/cmdc.201402075

Reference yield:

: 1624283-64-2
ethyl 2-[4-(4-methoxyphenylamino)-2-oxopyridin-1(2H)-yl]acetate

: 1624283-49-3
2-[4-(4-methoxyphenylamino)-2-oxo-2H-pyridin-1-yl]-N-isopentylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: lithium hydroxide / ethanol; water / 4 h / 0 - 20 °C

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / -15 - 20 °C

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In ethanol; dichloromethane; water;
DOI:10.1002/cmdc.201402075