1-(6-chloro-4-(4-methoxyphenyl)-2H-pyrano[4,3,2-cd]indol-5(3H)-yl)ethanone

Base Information

• Chemical Name: 1-(6-chloro-4-(4-methoxyphenyl)-2H-pyrano[4,3,2-cd]indol-5(3H)-yl)ethanone
• CAS No.: 1616469-80-7
• Molecular Formula: C₁₉H₁₆ClNO₃
• Molecular Weight: 341.794

Synonyms:1-(6-chloro-4-(4-methoxyphenyl)-2H-pyrano[4,3,2-cd]indol-5(3H)-yl)ethanone

Chemical Property of 1-(6-chloro-4-(4-methoxyphenyl)-2H-pyrano[4,3,2-cd]indol-5(3H)-yl)ethanone

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Technology Process of 1-(6-chloro-4-(4-methoxyphenyl)-2H-pyrano[4,3,2-cd]indol-5(3H)-yl)ethanone

There total 2 articles about 1-(6-chloro-4-(4-methoxyphenyl)-2H-pyrano[4,3,2-cd]indol-5(3H)-yl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

C19H18ClNO3 (1616469-63-6) → 1-(4-(4-methoxyphenyl)-2H-pyrano[4,3,2-cd]indol-5(3H)-yl)ethanone (1616469-65-8) + 1-(6-chloro-4-(4-methoxyphenyl)-2H-pyrano[4,3,2-cd]indol-5(3H)-yl)ethanone (1616469-80-7)

Guidance literature:

With silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper(II) acetate monohydrate; In tert-Amyl alcohol; at 120 ℃; for 1h; Glovebox;

DOI:10.1039/c4cc02398f

Reference yield: 29.0%

C19H18ClNO3 (1616469-63-6) → 1-(6-chloro-4-(4-methoxyphenyl)-2H-pyrano[4,3,2-cd]indol-5(3H)-yl)ethanone (1616469-80-7)

Guidance literature:

With tris(acetonitrile)(η5-pentamethylcyclopentadienyl)rhodium(III) hexafluoroantimonate; oxygen; copper(II) acetate monohydrate; In acetone; at 20 ℃; for 16h;

DOI:10.1039/c4cc02947j

upstream raw materials:

C₁₉H₁₈ClNO₃

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