(1'S,3'R,4'R,5'S)-3'-(benzoyloxy)-4'-[(benzoyloxy)methyl]-1'-(5-methyl-2,4-(1H,3H)-dioxopyrimidin-1-yl)bicyclo[3.1.0]hexane

Base Information

Chemical Name:(1'S,3'R,4'R,5'S)-3'-(benzoyloxy)-4'-[(benzoyloxy)methyl]-1'-(5-methyl-2,4-(1H,3H)-dioxopyrimidin-1-yl)bicyclo[3.1.0]hexane
CAS No.:205868-81-1
Molecular Formula:C₂₆H₂₄N₂O₆
Molecular Weight:460.486
Hs Code.:

Synonyms:(1'S,3'R,4'R,5'S)-3'-(benzoyloxy)-4'-[(benzoyloxy)methyl]-1'-(5-methyl-2,4-(1H,3H)-dioxopyrimidin-1-yl)bicyclo[3.1.0]hexane

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Chemical Property of (1'S,3'R,4'R,5'S)-3'-(benzoyloxy)-4'-[(benzoyloxy)methyl]-1'-(5-methyl-2,4-(1H,3H)-dioxopyrimidin-1-yl)bicyclo[3.1.0]hexane

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Technology Process of (1'S,3'R,4'R,5'S)-3'-(benzoyloxy)-4'-[(benzoyloxy)methyl]-1'-(5-methyl-2,4-(1H,3H)-dioxopyrimidin-1-yl)bicyclo[3.1.0]hexane

There total 1 articles about (1'S,3'R,4'R,5'S)-3'-(benzoyloxy)-4'-[(benzoyloxy)methyl]-1'-(5-methyl-2,4-(1H,3H)-dioxopyrimidin-1-yl)bicyclo[3.1.0]hexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.6%

: 65-85-0,8013-63-6
benzoic acid

: 156044-00-7
(S)-Methanocarba-Thymidine

: 205868-81-1
(1'S,3'R,4'R,5'S)-3'-(benzoyloxy)-4'-[(benzoyloxy)methyl]-1'-(5-methyl-2,4-(1H,3H)-dioxopyrimidin-1-yl)bicyclo[3.1.0]hexane

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In acetonitrile; benzene; for 12h; Ambient temperature;
DOI:10.1021/ja973535+

Reference yield:

: 205868-81-1
(1'S,3'R,4'R,5'S)-3'-(benzoyloxy)-4'-[(benzoyloxy)methyl]-1'-(5-methyl-2,4-(1H,3H)-dioxopyrimidin-1-yl)bicyclo[3.1.0]hexane

: 205868-85-5
Benzoic acid (1S,2S,3S,5S)-3-azido-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-bicyclo[3.1.0]hex-2-ylmethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: K₂CO₃

2: pyridine / 0 °C

3: Et₃N, DMAP

4: LiN₃ / dimethylformamide / 80 °C

With pyridine; dmap; lithium azide; potassium carbonate; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1080/07328319808004726

Reference yield:

: 205868-81-1
(1'S,3'R,4'R,5'S)-3'-(benzoyloxy)-4'-[(benzoyloxy)methyl]-1'-(5-methyl-2,4-(1H,3H)-dioxopyrimidin-1-yl)bicyclo[3.1.0]hexane

: 205868-84-4
Benzoic acid (1S,2R,3R,5S)-3-methanesulfonyloxy-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-bicyclo[3.1.0]hex-2-ylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃

2: pyridine / 0 °C

3: Et₃N, DMAP

With pyridine; dmap; potassium carbonate; triethylamine;
DOI:10.1080/07328319808004726