Benzenepropanoic acid, -alpha-,4-dimethyl--ba--methylene- (9CI)

Base Information

Chemical Name:Benzenepropanoic acid, -alpha-,4-dimethyl--ba--methylene- (9CI)
CAS No.:253664-01-6
Molecular Formula:C₁₂H₁₄O₂
Molecular Weight:190.242
Hs Code.:
Mol file:253664-01-6.mol

Synonyms:Benzenepropanoicacid,-alpha-,4-dimethyl--bta--methylene-(9CI);Benzenepropanoic acid, -alpha-,4-dimethyl--ba--methylene- (9CI)

Suppliers and Price of Benzenepropanoic acid, -alpha-,4-dimethyl--ba--methylene- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Benzenepropanoic acid, -alpha-,4-dimethyl--ba--methylene- (9CI)

Chemical Property:

PSA：37.30000
LogP:2.72890

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzenepropanoic acid, -alpha-,4-dimethyl--ba--methylene- (9CI)

There total 2 articles about Benzenepropanoic acid, -alpha-,4-dimethyl--ba--methylene- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 253663-98-8
2-methyl-3-p-tolylbut-3-enoic acid ethyl ester

: 253664-01-6
2-methyl-3-p-tolylbut-3-enoic acid

Guidance literature:: With potassium hydroxide; In ethanol; water; at 25 ℃; for 2h;
DOI:10.1016/S0040-4020(99)00826-1

Reference yield:

: 122-00-9
para-methylacetophenone

: 253664-01-6
2-methyl-3-p-tolylbut-3-enoic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: Zn; iodine / diethyl ether / 3 h / Heating

1.2: 97 percent / HCl / diethyl ether; H₂O

2.1: 20.4 g / KOH / H₂O; ethanol / 2 h / 25 °C

With potassium hydroxide; iodine; zinc; In diethyl ether; ethanol; water; 1.1: Condensation / 1.2: Elimination / 2.1: Hydrolysis;
DOI:10.1016/S0040-4020(99)00826-1