Z-N-ME-THR-OH CHA

Base Information

• Chemical Name: Z-N-ME-THR-OH CHA
• CAS No.: 253595-72-1
• Molecular Formula: C13H17 N O5
• Molecular Weight: 267.282
• Mol file: 253595-72-1.mol

Synonyms:Z-N-ME-THR-OH;Z-N-ME-THR-OH CHA;Z-L-METHR-OH;Z-N-METHYL-L-THREONINE;Z-N-MET-THR-OH CHA;N-ALPHA-BENZYLOXYCARBONYL-N-ALPHA-METHYL-L-THREONINE

Chemical Property of Z-N-ME-THR-OH CHA

Chemical Property:

• PSA: 87.07000
• LogP: 1.08900
• Storage Temp.: Store at RT.

Purity/Quality:

98%Min ^*data from raw suppliers

Z-N-methyl-L-threonine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Z-N-ME-THR-OH CHA

There total 2 articles about Z-N-ME-THR-OH CHA which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

(2S,3R)-3-Acetoxy-2-(benzyloxycarbonyl-methyl-amino)-butyric acid; compound with dicyclohexyl-amine (519156-38-8) → (2S,3R)-2-((benzyloxycarbonyl)(methyl)amino)-3-hydroxybutanoic acid (253595-72-1)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; at 60 ℃; for 30h;

DOI:10.1071/CH06148

Reference yield:

C13H17NO5*C12H23N → (2S,3R)-2-((benzyloxycarbonyl)(methyl)amino)-3-hydroxybutanoic acid (253595-72-1)

Guidance literature:

With sulfuric acid; In water; ethyl acetate;

Reference yield: 69.0%

Abu-Sar-O-(t-Bu) (117194-66-8) + (2S,3R)-2-((benzyloxycarbonyl)(methyl)amino)-3-hydroxybutanoic acid (253595-72-1) → Z-(Me)Thr(t-Bu)-Abu-Sar-O-(t-Bu) (117194-58-8)

Guidance literature:

With 4-methyl-morpholine; Diphenylphosphinic chloride; In tetrahydrofuran; 1.) -20 deg C, 1 h; 2.) rt, 24-48 h;

DOI:10.1016/S0040-4020(01)86731-4

upstream raw materials:

(2S,3R)-3-Acetoxy-2-(benzyloxycarbonyl-methyl-amino)-butyric acid; compound with dicyclohexyl-amine

Downstream raw materials:

Z-(Me)Thr(t-Bu)-Abu-Sar-O-(t-Bu)

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