2-(4-bromophenyl)-2-(tert-butyl(hydroxy)amino)-N,N-dimethylethanethioamide

Base Information

Chemical Name:2-(4-bromophenyl)-2-(tert-butyl(hydroxy)amino)-N,N-dimethylethanethioamide
CAS No.:1612163-30-0
Molecular Formula:C₁₄H₂₁BrN₂OS
Molecular Weight:345.304
Hs Code.:

Synonyms:2-(4-bromophenyl)-2-(tert-butyl(hydroxy)amino)-N,N-dimethylethanethioamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(4-bromophenyl)-2-(tert-butyl(hydroxy)amino)-N,N-dimethylethanethioamide

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Technology Process of 2-(4-bromophenyl)-2-(tert-butyl(hydroxy)amino)-N,N-dimethylethanethioamide

There total 2 articles about 2-(4-bromophenyl)-2-(tert-butyl(hydroxy)amino)-N,N-dimethylethanethioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 758-16-7
N,N-dimethylthioformamide

: 76790-28-8,127896-05-3
N-<(4-Bromophenyl)methylene>-2-methyl-2-propanamine N-oxide

: 1612163-30-0
2-(4-bromophenyl)-2-(tert-butyl(hydroxy)amino)-N,N-dimethylethanethioamide

Guidance literature:: With lithium diisopropyl amide; In toluene; at -78 ℃; for 0.333333h;
DOI:10.1021/jo500848a

Reference yield:

: 1122-91-4
4-bromo-benzaldehyde

: 1612163-30-0
2-(4-bromophenyl)-2-(tert-butyl(hydroxy)amino)-N,N-dimethylethanethioamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate / dichloromethane / 20 °C

2: lithium diisopropyl amide / toluene / 0.33 h / -78 °C

With sodium carbonate; lithium diisopropyl amide; In dichloromethane; toluene;
DOI:10.1021/jo500848a