6-(2,6-diethoxyphenyl)-1-(4-methoxybenzyl)-1,6-dihydropyridin-2(3H)-one

Base Information

Chemical Name:6-(2,6-diethoxyphenyl)-1-(4-methoxybenzyl)-1,6-dihydropyridin-2(3H)-one
CAS No.:1421692-74-1
Molecular Formula:C₂₃H₂₇NO₄
Molecular Weight:381.472
Hs Code.:

Synonyms:6-(2,6-diethoxyphenyl)-1-(4-methoxybenzyl)-1,6-dihydropyridin-2(3H)-one

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Chemical Property of 6-(2,6-diethoxyphenyl)-1-(4-methoxybenzyl)-1,6-dihydropyridin-2(3H)-one

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Technology Process of 6-(2,6-diethoxyphenyl)-1-(4-methoxybenzyl)-1,6-dihydropyridin-2(3H)-one

There total 4 articles about 6-(2,6-diethoxyphenyl)-1-(4-methoxybenzyl)-1,6-dihydropyridin-2(3H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 915770-09-1
1-(4-methoxybenzyl)-3,4-dihydropyridin-2(1H)-one

: 82935-36-2
2,6-diethoxybenzoic acid

: 1421692-74-1
6-(2,6-diethoxyphenyl)-1-(4-methoxybenzyl)-1,6-dihydropyridin-2(3H)-one

Guidance literature:: With silver (II) carbonate; palladium diacetate; propionic acid; triphenylphosphine; In N,N-dimethyl-formamide; at 80 ℃; for 24h;
DOI:10.1021/ol303497q

Reference yield:

: 1121-89-7
piperidine-2,6-dione

: 1421692-74-1
6-(2,6-diethoxyphenyl)-1-(4-methoxybenzyl)-1,6-dihydropyridin-2(3H)-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetra-(n-butyl)ammonium iodide; potassium carbonate / acetone / 12 h

2.1: Super-Hydride? / toluene; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

2.2: 2 h / 20 °C / Inert atmosphere

3.1: palladium diacetate; silver (II) carbonate; triphenylphosphine; propionic acid / N,N-dimethyl-formamide / 24 h / 80 °C

With silver (II) carbonate; palladium diacetate; tetra-(n-butyl)ammonium iodide; potassium carbonate; propionic acid; triphenylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1021/ol303497q

Reference yield:

: 1037681-49-4
1-[(4-methoxyphenyl)methyl]-2,6-piperidinedione

: 1421692-74-1
6-(2,6-diethoxyphenyl)-1-(4-methoxybenzyl)-1,6-dihydropyridin-2(3H)-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: Super-Hydride? / toluene; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: 2 h / 20 °C / Inert atmosphere

2.1: palladium diacetate; silver (II) carbonate; triphenylphosphine; propionic acid / N,N-dimethyl-formamide / 24 h / 80 °C

With silver (II) carbonate; palladium diacetate; propionic acid; triphenylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol303497q