6-(4-phenyl-5-thioxo-s-triazolin-3-yl)-4-methyl-2-phenyl-5-(1-pyrryl)-thieno[2,3-d]pyrimidine

Base Information

Chemical Name:6-(4-phenyl-5-thioxo-s-triazolin-3-yl)-4-methyl-2-phenyl-5-(1-pyrryl)-thieno[2,3-d]pyrimidine
CAS No.:487005-30-1
Molecular Formula:C₂₅H₁₈N₆S₂
Molecular Weight:466.59
Hs Code.:

Synonyms:6-(4-phenyl-5-thioxo-s-triazolin-3-yl)-4-methyl-2-phenyl-5-(1-pyrryl)-thieno[2,3-d]pyrimidine

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Chemical Property of 6-(4-phenyl-5-thioxo-s-triazolin-3-yl)-4-methyl-2-phenyl-5-(1-pyrryl)-thieno[2,3-d]pyrimidine

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Technology Process of 6-(4-phenyl-5-thioxo-s-triazolin-3-yl)-4-methyl-2-phenyl-5-(1-pyrryl)-thieno[2,3-d]pyrimidine

There total 5 articles about 6-(4-phenyl-5-thioxo-s-triazolin-3-yl)-4-methyl-2-phenyl-5-(1-pyrryl)-thieno[2,3-d]pyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 487005-29-8
1-(4-methyl-2-phenyl-5-(1-pyrryl)-thieno[2,3-d]pyrimidin-6-yl)carbonyl-4-phenylthiosemicarbazide

: 487005-30-1
6-(4-phenyl-5-thioxo-s-triazolin-3-yl)-4-methyl-2-phenyl-5-(1-pyrryl)-thieno[2,3-d]pyrimidine

Guidance literature:: With sodium hydroxide; for 4h; Heating;
DOI:10.1080/10426500210243

Reference yield:

: 128529-81-7
3-Amino-4-methyl-6-phenyl-thieno<2,3-d>pyrimidin-2-carbonsaeureethylester

: 487005-30-1
6-(4-phenyl-5-thioxo-s-triazolin-3-yl)-4-methyl-2-phenyl-5-(1-pyrryl)-thieno[2,3-d]pyrimidine

Guidance literature:: Multi-step reaction with 4 steps

1: 81 percent / acetic acid / 1 h / Heating

2: 79 percent / hydrazine hydrate; pyridine / 3 h / Heating

3: 90 percent / ethanol / 3 h / Heating

4: 75 percent / aq. NaOH / 4 h / Heating

With pyridine; sodium hydroxide; hydrazine hydrate; In ethanol; acetic acid;
DOI:10.1080/10426500210243

Reference yield:

: 2228-12-8
6-methyl-4-phenyl-2-thioxo-1,2-dihydropyrimidine-5-carbonitrile

: 487005-30-1
6-(4-phenyl-5-thioxo-s-triazolin-3-yl)-4-methyl-2-phenyl-5-(1-pyrryl)-thieno[2,3-d]pyrimidine

Guidance literature:: Multi-step reaction with 5 steps

1: 80 percent / K₂CO₃ / ethanol / 3 h / Heating

2: 81 percent / acetic acid / 1 h / Heating

3: 79 percent / hydrazine hydrate; pyridine / 3 h / Heating

4: 90 percent / ethanol / 3 h / Heating

5: 75 percent / aq. NaOH / 4 h / Heating

With pyridine; sodium hydroxide; potassium carbonate; hydrazine hydrate; In ethanol; acetic acid;
DOI:10.1080/10426500210243