C₃₄H₂₂N₂O₉

Base Information

• Chemical Name: C₃₄H₂₂N₂O₉
• CAS No.: 910656-88-1
• Molecular Formula: C₃₄H₂₂N₂O₉
• Molecular Weight: 602.557
• Mol file: 910656-88-1.mol

Synonyms:C₃₄H₂₂N₂O₉

Chemical Property of C₃₄H₂₂N₂O₉

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₄H₂₂N₂O₉

There total 1 articles about C₃₄H₂₂N₂O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

1-bromomethyl-4-nitro-benzene (100-11-8) + fluorescein free acid (518-45-6) → C34H22N2O9 (910656-88-1)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; for 18h; Reflux;

DOI:10.1016/j.carres.2011.06.001

Reference yield: 70.0%

C34H22N2O9 (910656-88-1) → C34H26N2O5 (1333505-22-8)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; for 25h;

DOI:10.1016/j.carres.2011.06.001

Reference yield:

C34H22N2O9 (910656-88-1) → C60H54N2O15 (1333505-29-5)

Guidance literature:

Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 25 h

2: methanol / 6 h / 20 °C

With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; methanol;

DOI:10.1016/j.carres.2011.06.001

upstream raw materials:

1-bromomethyl-4-nitro-benzene

fluorescein free acid

Downstream raw materials:

C₃₄H₂₆N₂O₅

C₆₀H₅₄N₂O₁₅