C₂₈H₂₇⁽²⁾H₁₀N₅O₃Si

Base Information

Chemical Name:C₂₈H₂₇⁽²⁾H₁₀N₅O₃Si
CAS No.:1346245-61-1
Molecular Formula:C₂₈H₃₇N₅O₃Si
Molecular Weight:529.64
Hs Code.:

C<sub>28</sub>H<sub>27</sub><sup>(2)</sup>H<sub>10</sub>N<sub>5</sub>O<sub>3</sub>Si

Synonyms:C₂₈H₂₇⁽²⁾H₁₀N₅O₃Si

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Chemical Property of C₂₈H₂₇⁽²⁾H₁₀N₅O₃Si

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Technology Process of C₂₈H₂₇⁽²⁾H₁₀N₅O₃Si

There total 6 articles about C₂₈H₂₇⁽²⁾H₁₀N₅O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 86864-60-0
(2 bromoethoxy-1,1,2,2-d₄)(1,1-dimethylethyl)dimethyl-silane

: 1346245-60-0
C₂₀H₁₃⁽²⁾H₆N₅O₂

: 1346245-61-1
C₂₈H₂₇⁽²⁾H₁₀N₅O₃Si

Guidance literature:: C₂₀H₁₃⁽²⁾H₆N₅O₂; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 5 ℃; for 1h;

(2 bromoethoxy-1,1,2,2-d₄)(1,1-dimethylethyl)dimethyl-silane; In N,N-dimethyl-formamide; mineral oil; at 5 - 20 ℃; for 4h; Inert atmosphere;

Reference yield:

: 106120-04-1
5-bromoresorcinol

: 1346245-61-1
C₂₈H₂₇⁽²⁾H₁₀N₅O₃Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: caesium carbonate / acetonitrile / 18 h / 80 °C

2.1: sodium t-butanolate / palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,4-dioxane / 96 h / 100 °C / Inert atmosphere

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 5 °C

3.2: 4 h / 5 - 20 °C / Inert atmosphere

With sodium hydride; caesium carbonate; sodium t-butanolate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In 1,4-dioxane; N,N-dimethyl-formamide; acetonitrile; mineral oil;

Reference yield:

: 1185311-78-7
C₈H₃⁽²⁾H₆BrO₂

: 1346245-61-1
C₂₈H₂₇⁽²⁾H₁₀N₅O₃Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium t-butanolate / palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,4-dioxane / 96 h / 100 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 5 °C

2.2: 4 h / 5 - 20 °C / Inert atmosphere

With sodium hydride; sodium t-butanolate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In 1,4-dioxane; N,N-dimethyl-formamide; mineral oil;