(S)-2-O-benzyl-1-O-monochloroacetylglycerol

Base Information

Chemical Name:(S)-2-O-benzyl-1-O-monochloroacetylglycerol
CAS No.:126568-78-3
Molecular Formula:C₁₂H₁₅ClO₄
Molecular Weight:258.702
Hs Code.:

Synonyms:(S)-2-O-benzyl-1-O-monochloroacetylglycerol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-O-benzyl-1-O-monochloroacetylglycerol

Chemical Property:

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Technology Process of (S)-2-O-benzyl-1-O-monochloroacetylglycerol

There total 9 articles about (S)-2-O-benzyl-1-O-monochloroacetylglycerol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 126568-77-2
(S)-2-O-benzyl-1-O-monochloroacetyl-3-O-tritylglycerol

: 126568-78-3
(S)-2-O-benzyl-1-O-monochloroacetylglycerol

Guidance literature:: With acetic acid; at 80 ℃; for 1h;
DOI:10.1248/cpb.38.3347

Reference yield: 2.0%

: 105409-41-4
1,3-di-O-chloroacetyl-2-O-benzylglycerol

: 14690-00-7
2-O-benzylglycerol

: 126568-78-3
1-O-chloroacetyl-2-O-benzylglycerol

Guidance literature:: With phosphate buffer; pig liver esterase; In acetone; at 30 ℃;
DOI:10.1248/cpb.34.3440

Reference yield:

: 109429-01-8
(S)-2-(benzyloxy)-3-hydroxypropyl acetate

: 126568-78-3
(S)-2-O-benzyl-1-O-monochloroacetylglycerol

Guidance literature:: Multi-step reaction with 4 steps

1: 72.5 percent / pyridine

2: 77.4 percent / NH₄OH / methanol

3: 91.5 percent / Et₃N / CH₂Cl₂

4: 69 percent / 80 percent AcOH / H₂O

With pyridine; ammonium hydroxide; acetic acid; triethylamine; In methanol; dichloromethane; water;
DOI:10.1248/cpb.37.2258