34,38-dioxo-35,37-dimethoxy-36-(phenylmethoxy)-10,15,20,31-tetramethyl-3,7,23,27-tetraazaheptacyclo<27.3.1.1^3,7.1^8,12.1^13,17.1^18,22.1^23,27>octaconta-1(33),8(35),9,11,13(36),14,16,18(37),19,21,29,31-dodecaen-33-ol

Base Information

• Chemical Name: 34,38-dioxo-35,37-dimethoxy-36-(phenylmethoxy)-10,15,20,31-tetramethyl-3,7,23,27-tetraazaheptacyclo<27.3.1.1^3,7.1^8,12.1^13,17.1^18,22.1^23,27>octaconta-1(33),8(35),9,11,13(36),14,16,18(37),19,21,29,31-dodecaen-33-ol
• CAS No.: 84379-22-6
• Molecular Formula: C₄₇H₅₀N₄O₆
• Molecular Weight: 766.937

Synonyms:34,38-dioxo-35,37-dimethoxy-36-(phenylmethoxy)-10,15,20,31-tetramethyl-3,7,23,27-tetraazaheptacyclo<27.3.1.1^3,7.1^8,12.1^13,17.1^18,22.1^23,27>octaconta-1(33),8(35),9,11,13(36),14,16,18(37),19,21,29,31-dodecaen-33-ol

Chemical Property of 34,38-dioxo-35,37-dimethoxy-36-(phenylmethoxy)-10,15,20,31-tetramethyl-3,7,23,27-tetraazaheptacyclo<27.3.1.1^3,7.1^8,12.1^13,17.1^18,22.1^23,27>octaconta-1(33),8(35),9,11,13(36),14,16,18(37),19,21,29,31-dodecaen-33-ol

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Technology Process of 34,38-dioxo-35,37-dimethoxy-36-(phenylmethoxy)-10,15,20,31-tetramethyl-3,7,23,27-tetraazaheptacyclo<27.3.1.1^3,7.1^8,12.1^13,17.1^18,22.1^23,27>octaconta-1(33),8(35),9,11,13(36),14,16,18(37),19,21,29,31-dodecaen-33-ol

There total 12 articles about 34,38-dioxo-35,37-dimethoxy-36-(phenylmethoxy)-10,15,20,31-tetramethyl-3,7,23,27-tetraazaheptacyclo<27.3.1.1^3,7.1^8,12.1^13,17.1^18,22.1^23,27>octaconta-1(33),8(35),9,11,13(36),14,16,18(37),19,21,29,31-dodecaen-33-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

34,38-dioxo-33-(2-propenyl-1-oxy)35,37-dimethoxy-36-(phenylmethoxy)-10,15,20,31-tetramethyl-3,7,23,27-tetraazaheptacyclo<27.3.1.13,7.18,12.113,17.118,22.123,27>octaconta-1(33),8(35),9,11,13(36),14,16,18(37),19,21,29,31-dodecaene (84379-21-5) → 34,38-dioxo-35,37-dimethoxy-36-(phenylmethoxy)-10,15,20,31-tetramethyl-3,7,23,27-tetraazaheptacyclo<27.3.1.13,7.18,12.113,17.118,22.123,27>octaconta-1(33),8(35),9,11,13(36),14,16,18(37),19,21,29,31-dodecaen-33-ol (84379-22-6)

Guidance literature:

With toluene-4-sulfonic acid; palladium on activated charcoal; In ethanol;

DOI:10.1039/c39820001219

Reference yield:

1-(2-propenyl-1-oxy)-2,6-(dihydroxymethyl)-4-methylbenzene (7259-92-9) → 34,38-dioxo-35,37-dimethoxy-36-(phenylmethoxy)-10,15,20,31-tetramethyl-3,7,23,27-tetraazaheptacyclo<27.3.1.13,7.18,12.113,17.118,22.123,27>octaconta-1(33),8(35),9,11,13(36),14,16,18(37),19,21,29,31-dodecaen-33-ol (84379-22-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 54 percent / PBr₃

2: 41 percent / NaH / tetrahydrofuran / -78 deg C to reflux

3: 25 percent / p-TosOH / 10percent Pd-C / ethanol

With phosphorus tribromide; sodium hydride; toluene-4-sulfonic acid; palladium on activated charcoal; In tetrahydrofuran; ethanol;

DOI:10.1039/c39820001219

Reference yield:

2,2''-dimethoxy-2'-(phenylmethoxy)-3,3''-dicarboxy-5,5',5''-trimethyl-1,1':3',1''-terphenyl (84379-28-2) → 34,38-dioxo-35,37-dimethoxy-36-(phenylmethoxy)-10,15,20,31-tetramethyl-3,7,23,27-tetraazaheptacyclo<27.3.1.13,7.18,12.113,17.118,22.123,27>octaconta-1(33),8(35),9,11,13(36),14,16,18(37),19,21,29,31-dodecaen-33-ol (84379-22-6)

Guidance literature:

Multi-step reaction with 5 steps

2: base

3: 89 percent / t-BuOK / 2-methyl-propan-2-ol

4: 41 percent / NaH / tetrahydrofuran / -78 deg C to reflux

5: 25 percent / p-TosOH / 10percent Pd-C / ethanol

With potassium tert-butylate; sodium hydride; toluene-4-sulfonic acid; palladium on activated charcoal; In tetrahydrofuran; ethanol; tert-butyl alcohol;

DOI:10.1039/c39820001219

upstream raw materials:

34,38-dioxo-33-(2-propenyl-1-oxy)35,37-dimethoxy-36-(phenylmethoxy)-10,15,20,31-tetramethyl-3,7,23,27-tetraazaheptacyclo<27.3.1.1^3,7.1^8,12.1^13,17.1^18,22.1^23,27>octaconta-1(33),8(35),9,11,13(36),14,16,18(37),19,21,29,31-dodecaene

2,6-bis(hydroxymethyl)-4-methylphenol

1-(2-propenyl-1-oxy)-2,6-(dihydroxymethyl)-4-methylbenzene

1-(2-propenyl-1-oxy)-2,6-bis(bromomethyl)-4-methylbenzene

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