allyl 2-O-acetyl-4-O-benzyl-6-O-tert-butyldiphenylsilyl-α-D-mannopyranoside

Base Information

• Chemical Name: allyl 2-O-acetyl-4-O-benzyl-6-O-tert-butyldiphenylsilyl-α-D-mannopyranoside
• CAS No.: 1430237-14-1
• Molecular Formula: C₃₄H₄₂O₇Si
• Molecular Weight: 590.789

Synonyms:allyl 2-O-acetyl-4-O-benzyl-6-O-tert-butyldiphenylsilyl-α-D-mannopyranoside

Chemical Property of allyl 2-O-acetyl-4-O-benzyl-6-O-tert-butyldiphenylsilyl-α-D-mannopyranoside

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Technology Process of allyl 2-O-acetyl-4-O-benzyl-6-O-tert-butyldiphenylsilyl-α-D-mannopyranoside

There total 1 articles about allyl 2-O-acetyl-4-O-benzyl-6-O-tert-butyldiphenylsilyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

allyl 4-O-benzyl-6-O-tert-butyldiphenylsilyl-α-D-mannopyranoside + Triethyl orthoacetate (78-39-7) → allyl 2-O-acetyl-4-O-benzyl-6-O-tert-butyldiphenylsilyl-α-D-mannopyranoside (1430237-14-1)

Guidance literature:

With camphor-10-sulfonic acid; In acetonitrile; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1002/chem.201705511

Reference yield: 100.0%

allyl 2-O-acetyl-4-O-benzyl-6-O-tert-butyldiphenylsilyl-α-D-mannopyranoside (1430237-14-1) + thioethyl 2,3,4-tri-O-benzyl-6-O-(2-naphthylmethyl)-D-galactopyranoside → C71H76O12Si

Guidance literature:

allyl 2-O-acetyl-4-O-benzyl-6-O-tert-butyldiphenylsilyl-α-D-mannopyranoside; thioethyl 2,3,4-tri-O-benzyl-6-O-(2-naphthylmethyl)-D-galactopyranoside; With N-iodo-succinimide; In diethyl ether; for 0.0833333h; Inert atmosphere; Molecular sieve;

With trimethylsilyl trifluoromethanesulfonate; In diethyl ether; at -11 ℃;

DOI:10.1002/chem.201705511

Reference yield: 83.0%

allyl 2-O-acetyl-4-O-benzyl-6-O-tert-butyldiphenylsilyl-α-D-mannopyranoside (1430237-14-1) + ethyl 2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl-(1->6)-2,3,4-tri-O-benzyl-1-thio-β-D-galactopyranoside (143995-72-6) → C95H104O17Si (1430237-15-2)

Guidance literature:

With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; N,N-dimethyl-formamide; In thiophene; toluene; at 0 ℃; Molecular sieve; Sonication;

DOI:10.1039/c2sc21515b

upstream raw materials:

Triethyl orthoacetate

Downstream raw materials:

C₉₅H₁₀₄O₁₇Si

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