C₁₃H₁₆BrNO

Base Information

Chemical Name:C₁₃H₁₆BrNO
CAS No.:1446478-57-4
Molecular Formula:C₁₃H₁₆BrNO
Molecular Weight:282.18
Hs Code.:

Synonyms:C₁₃H₁₆BrNO

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Chemical Property of C₁₃H₁₆BrNO

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Technology Process of C₁₃H₁₆BrNO

There total 2 articles about C₁₃H₁₆BrNO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1446478-56-3
C₁₀H₉BrO₂

: 107-11-9,30551-89-4
1-amino-2-propene

: 1446478-57-4
C₁₃H₁₆BrNO

: C₁₃H₁₆BrNO

Guidance literature:: With tetramethylammonium triacetoxyborohydride; In dichloromethane; acetic acid; at 23 ℃; Overall yield = 60 %;
DOI:10.1016/j.bmcl.2013.05.028

Reference yield:

: (3-bromobenzyl)magnesium bromide

: 1446478-57-4
C₁₃H₁₆BrNO

: C₁₃H₁₆BrNO

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether; dichloromethane / -78 °C

2: tetramethylammonium triacetoxyborohydride / dichloromethane; acetic acid / 23 °C

With tetramethylammonium triacetoxyborohydride; In diethyl ether; dichloromethane; acetic acid;
DOI:10.1016/j.bmcl.2013.05.028

Reference yield: 70.0%

: 1446478-57-4
C₁₃H₁₆BrNO

: C₁₀H₁₂BrNO

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1,3-dimethylbarbituric acid; In dichloromethane; at 23 ℃;
DOI:10.1016/j.bmcl.2013.05.028