1-(2,5-Bis-benzyloxy-phenyl)-4-tert-butyl-2,6,7-trioxa-bicyclo[2.2.2]octane

Base Information

Chemical Name:1-(2,5-Bis-benzyloxy-phenyl)-4-tert-butyl-2,6,7-trioxa-bicyclo[2.2.2]octane
CAS No.:123435-02-9
Molecular Formula:C₂₉H₃₂O₅
Molecular Weight:460.57
Hs Code.:

Synonyms:1-(2,5-Bis-benzyloxy-phenyl)-4-tert-butyl-2,6,7-trioxa-bicyclo[2.2.2]octane

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Chemical Property of 1-(2,5-Bis-benzyloxy-phenyl)-4-tert-butyl-2,6,7-trioxa-bicyclo[2.2.2]octane

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Technology Process of 1-(2,5-Bis-benzyloxy-phenyl)-4-tert-butyl-2,6,7-trioxa-bicyclo[2.2.2]octane

There total 3 articles about 1-(2,5-Bis-benzyloxy-phenyl)-4-tert-butyl-2,6,7-trioxa-bicyclo[2.2.2]octane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 123435-01-8
2,5-Bis-benzyloxy-benzoic acid 3-tert-butyl-oxetan-3-ylmethyl ester

: 123435-02-9
1-(2,5-Bis-benzyloxy-phenyl)-4-tert-butyl-2,6,7-trioxa-bicyclo[2.2.2]octane

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane;
DOI:10.1016/S0040-4039(01)80625-0

Reference yield:

: 94880-44-1
2,5-bis(benzyloxy)benzoyl chloride

: 123435-02-9
1-(2,5-Bis-benzyloxy-phenyl)-4-tert-butyl-2,6,7-trioxa-bicyclo[2.2.2]octane

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / pyridine / tetrahydrofuran

2: 70 percent / BF₃*Et₂O / CH₂Cl₂

With pyridine; boron trifluoride diethyl etherate; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(01)80625-0

Reference yield:

: 99250-47-2
3-t-butyl-3-hydroxymethyl-oxetane

: 123435-02-9
1-(2,5-Bis-benzyloxy-phenyl)-4-tert-butyl-2,6,7-trioxa-bicyclo[2.2.2]octane

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / pyridine / tetrahydrofuran

2: 70 percent / BF₃*Et₂O / CH₂Cl₂

With pyridine; boron trifluoride diethyl etherate; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(01)80625-0