Technology Process of 2,5-dimethoxy-N,N'-diphenyl-4-vinylaniline
There total 3 articles about 2,5-dimethoxy-N,N'-diphenyl-4-vinylaniline which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium tert-butylate; methyl-triphenylphosphonium iodide;
In
tetrahydrofuran;
at 20 ℃;
for 4h;
Inert atmosphere;
DOI:10.1039/b917065k
- Guidance literature:
-
Multi-step reaction with 3 steps
1: iodine; silver nitrate / methanol / 7 h / 20 °C
2: copper(I) oxide / N,N-dimethyl acetamide / 72 h / 190 °C
3: potassium tert-butylate; methyl-triphenylphosphonium iodide / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere
With
copper(I) oxide; potassium tert-butylate; iodine; methyl-triphenylphosphonium iodide; silver nitrate;
In
tetrahydrofuran; methanol; N,N-dimethyl acetamide;
DOI:10.1039/b917065k
- Guidance literature:
-
Multi-step reaction with 2 steps
1: copper(I) oxide / N,N-dimethyl acetamide / 72 h / 190 °C
2: potassium tert-butylate; methyl-triphenylphosphonium iodide / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere
With
copper(I) oxide; potassium tert-butylate; methyl-triphenylphosphonium iodide;
In
tetrahydrofuran; N,N-dimethyl acetamide;
DOI:10.1039/b917065k
