Technology Process of C24H34O5
There total 8 articles about C24H34O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydrogencarbonate;
In
methanol; water;
for 3h;
Heating;
DOI:10.1021/ja00019a051
- Guidance literature:
-
Multi-step reaction with 8 steps
1: (COCl)2, DMSO
4: 1.) n-BuLi, Cp2ZrCl2 / 1.) THF, -78 deg C to 20 deg C, overnight, 2.) -20 deg C, 3 h
5: 1.) n-BuLi, 2.) n-Bu4NF / 1.) THF, -78 deg C, 15 min, 2.) THF, 0 deg C, 5 min
6: PPTS / benzene
7: 1.) BH3*THF, 2.) 30percent H2O2, aq. NaOAc / 1.) THF, 20 deg C, 16 h, 2.) 50 deg C, 15 min
8: 76 percent / NaHCO3 / methanol; H2O / 3 h / Heating
With
n-butyllithium; zirconocene dichloride; borane-THF; oxalyl dichloride; tetrabutyl ammonium fluoride; dihydrogen peroxide; sodium acetate; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; dimethyl sulfoxide;
In
methanol; water; benzene;
DOI:10.1021/ja00019a051
- Guidance literature:
-
Multi-step reaction with 7 steps
3: 1.) n-BuLi, Cp2ZrCl2 / 1.) THF, -78 deg C to 20 deg C, overnight, 2.) -20 deg C, 3 h
4: 1.) n-BuLi, 2.) n-Bu4NF / 1.) THF, -78 deg C, 15 min, 2.) THF, 0 deg C, 5 min
5: PPTS / benzene
6: 1.) BH3*THF, 2.) 30percent H2O2, aq. NaOAc / 1.) THF, 20 deg C, 16 h, 2.) 50 deg C, 15 min
7: 76 percent / NaHCO3 / methanol; H2O / 3 h / Heating
With
n-butyllithium; zirconocene dichloride; borane-THF; tetrabutyl ammonium fluoride; dihydrogen peroxide; sodium acetate; pyridinium p-toluenesulfonate; sodium hydrogencarbonate;
In
methanol; water; benzene;
DOI:10.1021/ja00019a051
