2-(2-Methoxy-5-methyl-benzyl)-5-[1-(2-methoxy-5-methyl-phenyl)-meth-(Z)-ylidene]-hexanedioic acid dimethyl ester

Base Information

Chemical Name:2-(2-Methoxy-5-methyl-benzyl)-5-[1-(2-methoxy-5-methyl-phenyl)-meth-(Z)-ylidene]-hexanedioic acid dimethyl ester
CAS No.:101046-51-9
Molecular Formula:C₂₆H₃₂O₆
Molecular Weight:440.536
Hs Code.:

Synonyms:2-(2-Methoxy-5-methyl-benzyl)-5-[1-(2-methoxy-5-methyl-phenyl)-meth-(Z)-ylidene]-hexanedioic acid dimethyl ester

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Chemical Property of 2-(2-Methoxy-5-methyl-benzyl)-5-[1-(2-methoxy-5-methyl-phenyl)-meth-(Z)-ylidene]-hexanedioic acid dimethyl ester

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Technology Process of 2-(2-Methoxy-5-methyl-benzyl)-5-[1-(2-methoxy-5-methyl-phenyl)-meth-(Z)-ylidene]-hexanedioic acid dimethyl ester

There total 6 articles about 2-(2-Methoxy-5-methyl-benzyl)-5-[1-(2-methoxy-5-methyl-phenyl)-meth-(Z)-ylidene]-hexanedioic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: 101046-50-8
2-(2-Hydroxy-5-methyl-benzyl)-4-(6-methyl-2-oxo-2H-chromen-3-yl)-butyric acid

: 77-78-1
dimethyl sulfate

: 101046-52-0
2-(2-Methoxy-5-methyl-benzyl)-5-[1-(2-methoxy-5-methyl-phenyl)-meth-(Z)-ylidene]-hexanedioic acid

: 101046-51-9
2-(2-Methoxy-5-methyl-benzyl)-5-[1-(2-methoxy-5-methyl-phenyl)-meth-(Z)-ylidene]-hexanedioic acid dimethyl ester

Guidance literature:: With sodium hydroxide; for 0.5h; Heating;
DOI:10.1016/S0040-4020(01)96670-0

Reference yield: 11.0%

: 101046-50-8
2-(2-Hydroxy-5-methyl-benzyl)-4-(6-methyl-2-oxo-2H-chromen-3-yl)-butyric acid

: 101046-52-0
2-(2-Methoxy-5-methyl-benzyl)-5-[1-(2-methoxy-5-methyl-phenyl)-meth-(Z)-ylidene]-hexanedioic acid

: 101046-51-9
2-(2-Methoxy-5-methyl-benzyl)-5-[1-(2-methoxy-5-methyl-phenyl)-meth-(Z)-ylidene]-hexanedioic acid dimethyl ester

Guidance literature:: With sodium hydroxide; for 2h; Heating;
DOI:10.1016/S0040-4020(01)96670-0

Reference yield:

: 106-44-5
p-cresol

: 101046-51-9
2-(2-Methoxy-5-methyl-benzyl)-5-[1-(2-methoxy-5-methyl-phenyl)-meth-(Z)-ylidene]-hexanedioic acid dimethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / NaOH / ethanol; dimethylformamide / Heating

2: 82 percent / 1,2-dichloro-benzene; diethyl ether / 6 h / Heating

3: 50percent NaOH / 1.) heating, water, 10 min.; 2.) heating, 30 min

With sodium hydroxide; In diethyl ether; ethanol; N,N-dimethyl-formamide; 1,2-dichloro-benzene;
DOI:10.1016/S0040-4020(01)96670-0