Technology Process of C21H31NO3
There total 5 articles about C21H31NO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C28H45NO6S;
With
water; trifluoroacetic acid;
at 20 ℃;
for 1h;
With
triethylsilane;
In
water;
DOI:10.1016/j.tetlet.2012.05.009
- Guidance literature:
-
Multi-step reaction with 5 steps
1: dihydrogen peroxide; 9-bora-bicyclo[3.3.1]nonane; sodium hydroxide / dichloromethane
2: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran
3: tetrabutyl ammonium fluoride / tetrahydrofuran
4: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane
5: water; trifluoroacetic acid / 1 h / 20 °C
With
dmap; tetrabutyl ammonium fluoride; water; dihydrogen peroxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 9-bora-bicyclo[3.3.1]nonane; triphenylphosphine; trifluoroacetic acid; sodium hydroxide; diethylazodicarboxylate;
In
tetrahydrofuran; dichloromethane;
2: Mitsunobu reaction;
DOI:10.1016/j.tetlet.2012.05.009
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran
2: tetrabutyl ammonium fluoride / tetrahydrofuran
3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane
4: water; trifluoroacetic acid / 1 h / 20 °C
With
dmap; tetrabutyl ammonium fluoride; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triphenylphosphine; trifluoroacetic acid; diethylazodicarboxylate;
In
tetrahydrofuran; dichloromethane;
1: Mitsunobu reaction;
DOI:10.1016/j.tetlet.2012.05.009
