(S)-2-(1-(4-methoxyphenyl)propyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:(S)-2-(1-(4-methoxyphenyl)propyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:1589553-46-7
Molecular Formula:C₁₆H₂₅BO₃
Molecular Weight:276.184
Hs Code.:

Synonyms:(S)-2-(1-(4-methoxyphenyl)propyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Chemical Property of (S)-2-(1-(4-methoxyphenyl)propyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Technology Process of (S)-2-(1-(4-methoxyphenyl)propyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 3 articles about (S)-2-(1-(4-methoxyphenyl)propyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1589553-46-7
(S)-2-(1-(4-methoxyphenyl)propyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With ImPPA; cobalt(II) acetate; In diethyl ether; at 20 ℃; for 18h; Schlenk technique; Inert atmosphere;

Reference yield: 64.0%

: 1589553-45-6
(S)-1-(4-methoxyphenyl)propyl diisopropylcarbamate

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1589553-46-7
(S)-2-(1-(4-methoxyphenyl)propyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: (S)-1-(4-methoxyphenyl)propyl diisopropylcarbamate; With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; In diethyl ether; hexane; cyclohexane; at -78 ℃; for 1h; Inert atmosphere;

4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; In diethyl ether; hexane; cyclohexane; at -78 - 20 ℃; for 4h; stereospecific reaction; Inert atmosphere;
DOI:10.1039/c4cc00993b

Reference yield:

: 104-46-1,25086-72-0,63589-56-0
anethole

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1589553-46-7
(S)-2-(1-(4-methoxyphenyl)propyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: C₁₆H₂₅BO₃

Guidance literature:: With C₂₉H₃₃Cl₂CoN₃O; sodium tri-sec-butylborohydride; In tetrahydrofuran; at 25 ℃; for 5h; Overall yield = 69 %; enantioselective reaction; Inert atmosphere;
DOI:10.1021/acscatal.6b02278