N-Boc-L-Tyr(O-Disperse Red)-OPfp

Base Information

Chemical Name:N-Boc-L-Tyr(O-Disperse Red)-OPfp
CAS No.:371768-46-6
Molecular Formula:C₃₆H₃₄F₅N₅O₇
Molecular Weight:743.687
Hs Code.:

Synonyms:N-Boc-L-Tyr(O-Disperse Red)-OPfp

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Chemical Property of N-Boc-L-Tyr(O-Disperse Red)-OPfp

Chemical Property:

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Technology Process of N-Boc-L-Tyr(O-Disperse Red)-OPfp

There total 4 articles about N-Boc-L-Tyr(O-Disperse Red)-OPfp which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 2-tert-butoxycarbonylamino-3-[4-(2-{ethyl-[4-(4-nitro-phenylazo)-phenyl]-amino}-ethoxy)-phenyl]-propionic acid

: 371768-46-6
N-Boc-L-Tyr(O-Disperse Red)-OPfp

Guidance literature:: With N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane; at 20 ℃;
DOI:10.1002/1521-3765(20010803)7:15<3342::AID-CHEM3342>3.0.CO;2-7

Reference yield:

: 4326-36-7
(S)-N-(tert-butoxycarbonyl)tyrosine methyl ester

: 371768-46-6
N-Boc-L-Tyr(O-Disperse Red)-OPfp

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / Ph₃P; DEAD / toluene / 16 h / 20 °C

2: aq. NaOH / methanol; tetrahydrofuran / 20 °C

3: 2.63 g / EDC / CH₂Cl₂ / 20 °C

With sodium hydroxide; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; dichloromethane; toluene; 1: Mitsunobu reaction;
DOI:10.1002/1521-3765(20010803)7:15<3342::AID-CHEM3342>3.0.CO;2-7

Reference yield:

: 2872-52-8
disperse red 1

: 371768-46-6
N-Boc-L-Tyr(O-Disperse Red)-OPfp

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / Ph₃P; DEAD / toluene / 16 h / 20 °C

2: aq. NaOH / methanol; tetrahydrofuran / 20 °C

3: 2.63 g / EDC / CH₂Cl₂ / 20 °C

With sodium hydroxide; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; dichloromethane; toluene; 1: Mitsunobu reaction;
DOI:10.1002/1521-3765(20010803)7:15<3342::AID-CHEM3342>3.0.CO;2-7