Undec-10-enoic acid 1-(4-chloro-benzoylamino)-2-(4-chloro-phenyl)-2-oxo-ethyl ester

Base Information

• Chemical Name: Undec-10-enoic acid 1-(4-chloro-benzoylamino)-2-(4-chloro-phenyl)-2-oxo-ethyl ester
• CAS No.: 78010-62-5
• Molecular Formula: C₂₆H₂₉Cl₂NO₄
• Molecular Weight: 490.427

Synonyms:Undec-10-enoic acid 1-(4-chloro-benzoylamino)-2-(4-chloro-phenyl)-2-oxo-ethyl ester

Chemical Property of Undec-10-enoic acid 1-(4-chloro-benzoylamino)-2-(4-chloro-phenyl)-2-oxo-ethyl ester

Chemical Property:

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Technology Process of Undec-10-enoic acid 1-(4-chloro-benzoylamino)-2-(4-chloro-phenyl)-2-oxo-ethyl ester

There total 2 articles about Undec-10-enoic acid 1-(4-chloro-benzoylamino)-2-(4-chloro-phenyl)-2-oxo-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

10-undecenoic acid (112-38-9) + 4-Chloro-N-[1-chloro-2-(4-chloro-phenyl)-2-oxo-ethyl]-benzamide (78010-53-4) → Undec-10-enoic acid 1-(4-chloro-benzoylamino)-2-(4-chloro-phenyl)-2-oxo-ethyl ester (78010-62-5)

Guidance literature:

With triethylamine; In tetrahydrofuran; for 1h;

DOI:10.1002/ardp.19813140305

Reference yield:

4-Chloro-N-[2-(4-chloro-phenyl)-1-hydroxy-2-oxo-ethyl]-benzamide (78010-49-8) → Undec-10-enoic acid 1-(4-chloro-benzoylamino)-2-(4-chloro-phenyl)-2-oxo-ethyl ester (78010-62-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 88 percent / CHCl₃; tetrahydrofuran / 0.5 h / Heating

2: 73 percent / (C₂H₅)3N / tetrahydrofuran / 1 h

With triethylamine; In tetrahydrofuran; chloroform;

DOI:10.1002/ardp.19813140305

upstream raw materials:

10-undecenoic acid

4-Chloro-N-[1-chloro-2-(4-chloro-phenyl)-2-oxo-ethyl]-benzamide

4-Chloro-N-[2-(4-chloro-phenyl)-1-hydroxy-2-oxo-ethyl]-benzamide

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