3-(benzyloxy)-2-iodopropanal

Base Information

Chemical Name:3-(benzyloxy)-2-iodopropanal
CAS No.:1255516-92-7
Molecular Formula:C₁₀H₁₁IO₂
Molecular Weight:290.101
Hs Code.:

Synonyms:3-(benzyloxy)-2-iodopropanal

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Chemical Property of 3-(benzyloxy)-2-iodopropanal

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Technology Process of 3-(benzyloxy)-2-iodopropanal

There total 1 articles about 3-(benzyloxy)-2-iodopropanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 81028-03-7
(Z)-4-benzyloxy-but-2-en-1-ol

: 1255516-92-7
3-(benzyloxy)-2-iodopropanal

Guidance literature:: With [Ir(III)(η5-pentamethylcyclopentadienyl)(H2O)3](SO4); iodine; oxygen; sodium nitrite; In 2-methyltetrahydrofuran; water; at 20 ℃; for 48h; under 760.051 Torr; Sealed tube;
DOI:10.1002/adsc.201800661

Reference yield:

: 53431-72-4
α-nitro cinnamate de methyle

: 1255516-92-7
3-(benzyloxy)-2-iodopropanal

: (4RS,5RS)-5-(benzyloxymethyl)-5-formyl-3-(methoxycarbonyl)-4-phenyl-4,5-dihydroisoxazole 2-oxide

Guidance literature:: With α,α-diphenyl-2-pyrrolidinemethanol trimethylsilyl ether; triethylamine; In toluene; at 23 ℃; diastereoselective reaction;
DOI:10.1021/ol102181r

Reference yield:

: 53431-72-4
α-nitro cinnamate de methyle

: 1255516-92-7
3-(benzyloxy)-2-iodopropanal

: 1255516-97-2
(4S,5S)-5-(benzyloxymethyl)-5-formyl-3-(methoxycarbonyl)-4-phenyl-4,5-dihydroisoxazole 2-oxide

: (4RS,5SR)-5-(benzyloxymethyl)-5-formyl-3-(methoxycarbonyl)-4-phenyl-4,5-dihydroisoxazole 2-oxide

Guidance literature:: With (S)-2-(azidodiphenylmethyl)pyrrolidine; triethylamine; In toluene; at 23 ℃; for 14h; optical yield given as %ee; enantioselective reaction;
DOI:10.1021/ol102181r