C₁₈H₂₄O₃

Base Information

Chemical Name:C₁₈H₂₄O₃
CAS No.:1195988-28-3
Molecular Formula:C₁₈H₂₄O₃
Molecular Weight:288.387
Hs Code.:

C<sub>18</sub>H<sub>24</sub>O<sub>3</sub>

Synonyms:C₁₈H₂₄O₃

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Chemical Property of C₁₈H₂₄O₃

Chemical Property:

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Technology Process of C₁₈H₂₄O₃

There total 1 articles about C₁₈H₂₄O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1195988-17-0
C₁₅H₁₈O₃

: 2622-05-1
allylmagnesium bromide

: 1195988-28-3
C₁₈H₂₄O₃

Guidance literature:: allylmagnesium bromide; With copper(l) iodide; In tetrahydrofuran; at -40 ℃; for 0.5h;

C₁₅H₁₈O₃; In tetrahydrofuran; at -40 ℃; for 1.5h;
DOI:10.1021/ol902217q

Reference yield:

: 1195988-28-3
C₁₈H₂₄O₃

: 108-24-7
acetic anhydride

: 1195988-18-1
C₂₀H₂₆O₄

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 2.5h;
DOI:10.1021/ol902217q

Reference yield:

: 1195988-28-3
C₁₈H₂₄O₃

: C₃₂H₄₈O₆Si

: 1263144-07-5
C₃₂H₄₈O₆Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: dmap; triethylamine / 2.5 h / 20 °C

2.1: osmium(VIII) oxide; AD-mix-β; 1,4-bis(9-O-dihydroquinidine)phthalazine / water; tert-butyl alcohol / 70 h / 0 - 20 °C

3.1: silica-supported sodium periodate / dichloromethane / 0.67 h / 0 - 20 °C

4.1: tetrahydrofuran / 13.83 h / -40 °C

5.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.33 h / -78 °C

5.2: -78 - 20 °C

6.1: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2S,3S)-tartrate / dichloromethane / 44 h / -40 - -15 °C / Molecular sieve

6.2: 3 h / -15 - 20 °C

7.1: silver nitrate; triethylamine / tetrahydrofuran / 0.75 h / 0 °C

7.2: 15 h / 0 - 20 °C

8.1: camphor-10-sulfonic acid / methanol; dichloromethane / 2.5 h / 0 - 20 °C

9.1: dimethyl sulfoxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / 3 h / 20 °C

10.1: potassium hexamethylsilazane / 1,2-dimethoxyethane / 0.5 h / -75 - -65 °C

10.2: 3 h / -75 - 0 °C

With titanium(IV) isopropylate; tert.-butylhydroperoxide; dmap; osmium(VIII) oxide; diethyl (2S,3S)-tartrate; silica-supported sodium periodate; AD-mix-β; camphor-10-sulfonic acid; potassium hexamethylsilazane; diisobutylaluminium hydride; silver nitrate; dimethyl sulfoxide; 1,4-bis(9-O-dihydroquinidine)phthalazine; triethylamine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; hexane; dichloromethane; water; tert-butyl alcohol; 4.1: Wittig reaction / 6.1: Sharpless epoxidation / 10.1: Julia-Kocienski reaction / 10.2: Julia-Kocienski reaction;
DOI:10.1016/j.tet.2010.11.017