4,5-bis[3-[2-(2-(2-methoxyethoxy)ethoxy)ethoxy]-phenoxy]phthalonitrile

Base Information

Chemical Name:4,5-bis[3-[2-(2-(2-methoxyethoxy)ethoxy)ethoxy]-phenoxy]phthalonitrile
CAS No.:1415420-05-1
Molecular Formula:C₃₄H₄₀N₂O₁₀
Molecular Weight:636.699
Hs Code.:

Synonyms:4,5-bis[3-[2-(2-(2-methoxyethoxy)ethoxy)ethoxy]-phenoxy]phthalonitrile

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Chemical Property of 4,5-bis[3-[2-(2-(2-methoxyethoxy)ethoxy)ethoxy]-phenoxy]phthalonitrile

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Technology Process of 4,5-bis[3-[2-(2-(2-methoxyethoxy)ethoxy)ethoxy]-phenoxy]phthalonitrile

There total 2 articles about 4,5-bis[3-[2-(2-(2-methoxyethoxy)ethoxy)ethoxy]-phenoxy]phthalonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 245070-93-3
3-[2-(2-(2-methoxyethoxy)ethoxy)ethoxy]phenol

: 139152-08-2
4,5-dichlorophthalonitrile

: 1415420-05-1
4,5-bis[3-[2-(2-(2-methoxyethoxy)ethoxy)ethoxy]-phenoxy]phthalonitrile

Guidance literature:: With potassium carbonate; In N,N-dimethyl acetamide; at 120 ℃; for 2h; Inert atmosphere;
DOI:10.1142/S1088424612501222 DOI:10.1142/S1088424612501222

Reference yield:

: 112-35-6,95507-80-5
triethylene glucol monomethyl ether

: 1415420-05-1
4,5-bis[3-[2-(2-(2-methoxyethoxy)ethoxy)ethoxy]-phenoxy]phthalonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / tetrahydrofuran / 2 h / 5 °C

2: potassium carbonate / acetonitrile / 24 h / Reflux; Inert atmosphere

3: potassium carbonate / N,N-dimethyl acetamide / 2 h / 120 °C / Inert atmosphere

With potassium carbonate; sodium hydroxide; In tetrahydrofuran; N,N-dimethyl acetamide; acetonitrile;
DOI:10.1142/S1088424612501222 DOI:10.1142/S1088424612501222

Reference yield: 93.0%

: 1415420-05-1
4,5-bis[3-[2-(2-(2-methoxyethoxy)ethoxy)ethoxy]-phenoxy]phthalonitrile

: copper dichloride

: 1415420-04-0
2,3,9,10,16,17,23,24-octakis[3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenoxy]-phthalocyaninatocopper (II)

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In pentan-1-ol; for 24h; Reflux; Inert atmosphere;
DOI:10.1142/S1088424612501222 DOI:10.1142/S1088424612501222