1-(1.2.4-Triazol-1-yl)-1-(2.4-dichlorbenzyloximino)-3.3-dimethylbutan-2-on

Base Information

• Chemical Name: 1-(1.2.4-Triazol-1-yl)-1-(2.4-dichlorbenzyloximino)-3.3-dimethylbutan-2-on
• CAS No.: 83397-04-0
• Molecular Formula: C₁₅H₁₆Cl₂N₄O₂
• Molecular Weight: 355.224

Synonyms:1-(1.2.4-Triazol-1-yl)-1-(2.4-dichlorbenzyloximino)-3.3-dimethylbutan-2-on

Chemical Property of 1-(1.2.4-Triazol-1-yl)-1-(2.4-dichlorbenzyloximino)-3.3-dimethylbutan-2-on

Chemical Property:

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Technology Process of 1-(1.2.4-Triazol-1-yl)-1-(2.4-dichlorbenzyloximino)-3.3-dimethylbutan-2-on

There total 2 articles about 1-(1.2.4-Triazol-1-yl)-1-(2.4-dichlorbenzyloximino)-3.3-dimethylbutan-2-on which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.2%

2,4-Dichlorobenzyl chloride (94-99-5) + 1-(1.2.4-Triazol-1-yl)-1-oximino-3.3-dimethylbutanon-2 (83402-51-1) → 1-(1.2.4-Triazol-1-yl)-1-(2.4-dichlorbenzyloximino)-3.3-dimethylbutan-2-on (83397-04-0)

Guidance literature:

With potassium carbonate; potassium iodide; In acetonitrile; at 23 ℃; for 36h;

DOI:10.1515/znb-1982-0723

Reference yield:

3,3-dimethyl-1-(1,2,4-triazol-1-yl)-2-butanone (58905-32-1) → 1-(1.2.4-Triazol-1-yl)-1-(2.4-dichlorbenzyloximino)-3.3-dimethylbutan-2-on (83397-04-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) Na/EtOH, 2.) i-C₅H₉ONO / 2.) 22 deg C, 8 h

2: 93.2 percent / K₂CO₃, KI / acetonitrile / 36 h / 23 °C

With ethanol; sodium; potassium carbonate; potassium iodide; isopentyl nitrite; In acetonitrile;

DOI:10.1515/znb-1982-0723

Reference yield: 94.2%

1-(1.2.4-Triazol-1-yl)-1-(2.4-dichlorbenzyloximino)-3.3-dimethylbutan-2-on (83397-04-0) → 1-(1.2.4-Triazol-1-yl)-1-(2.4-dichlorbenzyloximino)-2-hydroxy-3.3-dimethylbutan

Guidance literature:

With sodium tetrahydroborate; In methanol; 1.) 0 deg C, 2 h; 2.) 22 deg C, 3 h;

DOI:10.1515/znb-1982-0723

upstream raw materials:

2,4-Dichlorobenzyl chloride

1-(1.2.4-Triazol-1-yl)-1-oximino-3.3-dimethylbutanon-2

3,3-dimethyl-1-(1,2,4-triazol-1-yl)-2-butanone

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