[MeC₆H₄N(-)SiMe₂N(CH₂CH₂P(i)Pr₂)2]CoI

Base Information

• Chemical Name: [MeC₆H₄N(-)SiMe₂N(CH₂CH₂P(i)Pr₂)2]CoI
• CAS No.: 1138164-54-1
• Molecular Formula: C₂₅H₄₉CoIN₂P₂Si
• Molecular Weight: 653.608

Synonyms:[MeC₆H₄N(-)SiMe₂N(CH₂CH₂P(i)Pr₂)2]CoI

Chemical Property of [MeC₆H₄N(-)SiMe₂N(CH₂CH₂P(i)Pr₂)2]CoI

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Technology Process of [MeC₆H₄N(-)SiMe₂N(CH₂CH₂P(i)Pr₂)2]CoI

There total 1 articles about [MeC₆H₄N(-)SiMe₂N(CH₂CH₂P(i)Pr₂)2]CoI which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

Li[MeC6H4N(-)SiMe2N(CH2CH2P(i)Pr2)2] + cobalt(II) iodide → [MeC6H4N(-)SiMe2N(CH2CH2P(i)Pr2)2]CoI (1138164-54-1)

Guidance literature:

In toluene; using Schlenk techniques; a soln. of Li-contg. compd. (4.2 mmol) was added dropwise to a suspn. of CoI2 (4.2 mmol) in toluene; the mixt. was stirred overnight; solvent was removed under vac.; compd. was dissolved in THF and filtered; an equal vol. of pentane was added; cooling at -40°C overnight;elem. anal.;

DOI:10.1021/ic802337t

Reference yield: 72.0%

[MeC6H4N(-)SiMe2N(CH2CH2P(i)Pr2)2]CoI (1138164-54-1) → [MeC6H4N(-)SiMe2N(CH2CH2P(i)Pr2)2]Co (1138164-55-2)

Guidance literature:

With KC₈; In 1,2-dimethoxyethane; using Schlenk techniques; a suspn. of KC8 (3.1 mmol) in DME was added toa soln. of Co-contg. compd. (3.0 mmol) in DME at -40°C; the mixt . was warmed to room temp. and stirred for 3 h; the solvent was removed under vac.; the compd. was extd. with pentane; the soln. was concd. and cooled at -40°C overnight; elem. anal.;

DOI:10.1021/ic802337t

Downstream raw materials:

[MeC₆H₄N(-)SiMe₂N(CH₂CH₂P(i)Pr₂)2]Co

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