2,2-dibenzylcyclobutanone

Base Information

Chemical Name:2,2-dibenzylcyclobutanone
CAS No.:1599438-42-2
Molecular Formula:C₁₈H₁₈O
Molecular Weight:250.34
Hs Code.:

Synonyms:2,2-dibenzylcyclobutanone

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Chemical Property of 2,2-dibenzylcyclobutanone

Chemical Property:

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Technology Process of 2,2-dibenzylcyclobutanone

There total 2 articles about 2,2-dibenzylcyclobutanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: C₆H₅N₂⁽¹⁺⁾*BF₄^(2-)

: 1599438-27-3
1-(1-phenylprop-2-en-2-yl)cyclopropanol

: 1599438-42-2
2,2-dibenzylcyclobutanone

Guidance literature:: With tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate; (triphenylphosphine)gold(I) chloride; In methanol; acetonitrile; at -78 - 20 ℃; for 6h; Inert atmosphere; Irradiation; Sealed tube;
DOI:10.1021/ja500716j

Reference yield:

: 60468-22-6
2-bromo-3-phenyl-propene

: 1599438-42-2
2,2-dibenzylcyclobutanone

Guidance literature:: Multi-step reaction with 2 steps

1.1: tert.-butyl lithium / tetrahydrofuran; pentane / 1.17 h / -78 °C / Inert atmosphere

1.2: 6 h / -78 - 20 °C

2.1: tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate; (triphenylphosphine)gold(I) chloride / methanol; acetonitrile / 6 h / -78 - 20 °C / Inert atmosphere; Irradiation; Sealed tube

With tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate; (triphenylphosphine)gold(I) chloride; tert.-butyl lithium; In tetrahydrofuran; methanol; acetonitrile; pentane;
DOI:10.1021/ja500716j