1-O-allyl-6-O-(2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)-2,3,4,5-tetra-O-benzyl-D-myo-inositol

Base Information

Chemical Name:1-O-allyl-6-O-(2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)-2,3,4,5-tetra-O-benzyl-D-myo-inositol
CAS No.:150772-58-0
Molecular Formula:C₅₀H₅₅N₃O₁₀
Molecular Weight:858.001
Hs Code.:

Synonyms:1-O-allyl-6-O-(2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)-2,3,4,5-tetra-O-benzyl-D-myo-inositol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-O-allyl-6-O-(2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)-2,3,4,5-tetra-O-benzyl-D-myo-inositol

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Technology Process of 1-O-allyl-6-O-(2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)-2,3,4,5-tetra-O-benzyl-D-myo-inositol

There total 5 articles about 1-O-allyl-6-O-(2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)-2,3,4,5-tetra-O-benzyl-D-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67857-23-2
4,6-di-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl bromide

: 150772-58-0
1-O-allyl-6-O-(2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)-2,3,4,5-tetra-O-benzyl-D-myo-inositol

Guidance literature:: Multi-step reaction with 2 steps

1: AgClO₄ / diethyl ether / 0.5 h / from -35 deg C to RT

2: NaOMe

With sodium methylate; silver perchlorate; In diethyl ether;
DOI:10.1021/ja00070a048

Reference yield:

: 132437-54-8
1-O-allyl-2,3,4,5-tetra-O-benzyl-D-myo-inositol

: 150772-58-0
1-O-allyl-6-O-(2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)-2,3,4,5-tetra-O-benzyl-D-myo-inositol

Guidance literature:: Multi-step reaction with 2 steps

1: AgClO₄ / diethyl ether / 0.5 h / from -35 deg C to RT

2: NaOMe

With sodium methylate; silver perchlorate; In diethyl ether;
DOI:10.1021/ja00070a048

Reference yield:

: Acetic acid (2R,3S,4R,5R,6R)-2-acetoxymethyl-6-((1S,2R,3S,4S,5R,6S)-2-allyloxy-3,4,5,6-tetrakis-benzyloxy-cyclohexyloxy)-5-azido-4-benzyloxy-tetrahydro-pyran-3-yl ester

: 1-O-allyl-6-O-(2-azido-3-O-benzyl-2-deoxy-β-D-glucopyranosyl)-2,3,4,5-tetra-O-acetyl-D-myo-inositol

: 150772-58-0
1-O-allyl-6-O-(2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)-2,3,4,5-tetra-O-benzyl-D-myo-inositol

Guidance literature:: With sodium methylate; In methanol; dichloromethane; for 1h; Yield given. Yields of byproduct given;
DOI:10.1021/ja00110a011