11,12-bis<(triisopropylsilyl)ethynyl>-1,4,7,10-tetraoxadispiro<4.0.4.2>dodec-11-ene

Base Information

Chemical Name:11,12-bis<(triisopropylsilyl)ethynyl>-1,4,7,10-tetraoxadispiro<4.0.4.2>dodec-11-ene
CAS No.:134816-81-2
Molecular Formula:C₃₀H₅₀O₄Si₂
Molecular Weight:530.896
Hs Code.:

Synonyms:11,12-bis<(triisopropylsilyl)ethynyl>-1,4,7,10-tetraoxadispiro<4.0.4.2>dodec-11-ene

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Chemical Property of 11,12-bis<(triisopropylsilyl)ethynyl>-1,4,7,10-tetraoxadispiro<4.0.4.2>dodec-11-ene

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Technology Process of 11,12-bis<(triisopropylsilyl)ethynyl>-1,4,7,10-tetraoxadispiro<4.0.4.2>dodec-11-ene

There total 1 articles about 11,12-bis<(triisopropylsilyl)ethynyl>-1,4,7,10-tetraoxadispiro<4.0.4.2>dodec-11-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 123002-93-7
3,4-diethynyl-3-cyclobutene-1,2-dione bis(ethylene ketal)

: 134816-67-4
(12-Ethynyl-1,4,7,10-tetraoxa-dispiro[4.0.4.2]dodec-11-en-11-ylethynyl)-triisopropyl-silane

: 134816-81-2
11,12-bis<(triisopropylsilyl)ethynyl>-1,4,7,10-tetraoxadispiro<4.0.4.2>dodec-11-ene

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, hexane, -78 deg C, 15 min, 2.) THF, hexane, 20 deg C, 30 min;
DOI:10.1021/ja00018a035