Technology Process of C16H23NO2S
There total 5 articles about C16H23NO2S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1,1'-bis-(diphenylphosphino)ferrocene; formic acid; palladium diacetate; triethylamine;
In
toluene;
at 120 ℃;
for 10h;
Inert atmosphere;
DOI:10.1021/ja201204g
- Guidance literature:
-
Multi-step reaction with 2 steps
1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran
2: 1,1'-bis-(diphenylphosphino)ferrocene; formic acid; palladium diacetate; triethylamine / toluene / 10 h / 120 °C / Inert atmosphere
With
1,1'-bis-(diphenylphosphino)ferrocene; formic acid; di-isopropyl azodicarboxylate; palladium diacetate; triethylamine; triphenylphosphine;
In
tetrahydrofuran; toluene;
1: Mitsunobu reaction;
DOI:10.1021/ja201204g
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium hydroxide / ethanol; water / Reflux
2.1: lithium aluminium tetrahydride / diethyl ether / 4.67 h / 20 °C
2.2: 0.5 h / 0 °C / Saturated solution
3.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran
4.1: 1,1'-bis-(diphenylphosphino)ferrocene; formic acid; palladium diacetate; triethylamine / toluene / 10 h / 120 °C / Inert atmosphere
With
1,1'-bis-(diphenylphosphino)ferrocene; lithium aluminium tetrahydride; formic acid; di-isopropyl azodicarboxylate; palladium diacetate; triethylamine; triphenylphosphine; potassium hydroxide;
In
tetrahydrofuran; diethyl ether; ethanol; water; toluene;
3.1: Mitsunobu reaction;
DOI:10.1021/ja201204g
