gem-dimethyl-5,5'-bis(phenyl(hydroxy)methyl)-2,2'-dipyrrylmethane

Base Information

Chemical Name:gem-dimethyl-5,5'-bis(phenyl(hydroxy)methyl)-2,2'-dipyrrylmethane
CAS No.:881921-37-5
Molecular Formula:C₂₅H₂₆N₂O₂
Molecular Weight:386.494
Hs Code.:

Synonyms:gem-dimethyl-5,5'-bis(phenyl(hydroxy)methyl)-2,2'-dipyrrylmethane

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Chemical Property of gem-dimethyl-5,5'-bis(phenyl(hydroxy)methyl)-2,2'-dipyrrylmethane

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Technology Process of gem-dimethyl-5,5'-bis(phenyl(hydroxy)methyl)-2,2'-dipyrrylmethane

There total 2 articles about gem-dimethyl-5,5'-bis(phenyl(hydroxy)methyl)-2,2'-dipyrrylmethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 591-51-5
phenyllithium

: 550316-46-6
5,5′-(propane-2,2-diyl)bis(1H-pyrrole-2-carbaldehyde)

: 881921-37-5
gem-dimethyl-5,5'-bis(phenyl(hydroxy)methyl)-2,2'-dipyrrylmethane

Guidance literature:: phenyllithium; 5,5′-(propane-2,2-diyl)bis(1H-pyrrole-2-carbaldehyde); In tetrahydrofuran; diethyl ether; cyclohexane; at -65 - 20 ℃; for 3h;

With water; In tetrahydrofuran; diethyl ether; cyclohexane; Further stages.;
DOI:10.1039/b518340e

Reference yield:

: 99840-54-7
5,5'-dimethyldipyrromethane

: 881921-37-5
gem-dimethyl-5,5'-bis(phenyl(hydroxy)methyl)-2,2'-dipyrrylmethane

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate

With trichlorophosphate; 1: |Vilsmeier-Haack Formylation;
DOI:10.1007/s12039-012-0315-4