[(2'S,3'S,4'R,5'S)-N-(tert-butyloxycarbonyl)-3',4'-O-dibenzyl-5'-(O-benzylmethyl)pyrrolidin-2'-yl]carbaldehyde

Base Information

Chemical Name:[(2'S,3'S,4'R,5'S)-N-(tert-butyloxycarbonyl)-3',4'-O-dibenzyl-5'-(O-benzylmethyl)pyrrolidin-2'-yl]carbaldehyde
CAS No.:943860-61-5
Molecular Formula:C₃₂H₃₇NO₆
Molecular Weight:531.649
Hs Code.:

Synonyms:[(2'S,3'S,4'R,5'S)-N-(tert-butyloxycarbonyl)-3',4'-O-dibenzyl-5'-(O-benzylmethyl)pyrrolidin-2'-yl]carbaldehyde

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Chemical Property of [(2'S,3'S,4'R,5'S)-N-(tert-butyloxycarbonyl)-3',4'-O-dibenzyl-5'-(O-benzylmethyl)pyrrolidin-2'-yl]carbaldehyde

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Technology Process of [(2'S,3'S,4'R,5'S)-N-(tert-butyloxycarbonyl)-3',4'-O-dibenzyl-5'-(O-benzylmethyl)pyrrolidin-2'-yl]carbaldehyde

There total 1 articles about [(2'S,3'S,4'R,5'S)-N-(tert-butyloxycarbonyl)-3',4'-O-dibenzyl-5'-(O-benzylmethyl)pyrrolidin-2'-yl]carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 943860-60-4
(2R,3S,4R,5S)-N-(tert-butyloxycarbonyl)-2-(hydroxymethyl)-3,4-O-dibenzyl-5-(O-benzylmethyl)pyrrolidine

: 943860-61-5
[(2'S,3'S,4'R,5'S)-N-(tert-butyloxycarbonyl)-3',4'-O-dibenzyl-5'-(O-benzylmethyl)pyrrolidin-2'-yl]carbaldehyde

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -78 - 20 ℃; for 1.33333h;
DOI:10.1055/s-2007-966022

Reference yield: 71.0%

: 943860-61-5
[(2'S,3'S,4'R,5'S)-N-(tert-butyloxycarbonyl)-3',4'-O-dibenzyl-5'-(O-benzylmethyl)pyrrolidin-2'-yl]carbaldehyde

: 1439-36-7
1-triphenylphosphoranylidene-2-propanone

: 943860-62-6
(E)-[(2'R,3'S,4'R,5'S)-N-(tert-butyloxycarbonyl)-3',4'-O-dibenzyl-5'-(O-benzylmethyl)pyrrolidin-2'-yl]but-3-en-2-one

Guidance literature:: In toluene; for 24h; Heating;
DOI:10.1055/s-2007-966022

Reference yield:

: 943860-61-5
[(2'S,3'S,4'R,5'S)-N-(tert-butyloxycarbonyl)-3',4'-O-dibenzyl-5'-(O-benzylmethyl)pyrrolidin-2'-yl]carbaldehyde

: 943860-63-7
C₃₅H₄₃NO₆

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / toluene / 24 h / Heating

2: H₂ / Pd/C / methanol / 12 h / 750.08 Torr

With hydrogen; palladium on activated charcoal; In methanol; toluene; 1: Wittig reaction;
DOI:10.1055/s-2007-966022