allyl (methyl 2,3-di-O-benzoyl-4-O-tert-butyldimethylsilyl-β-D-glucopyranosyluronate)-(1->3)-(2-deoxy-2-acetamido-β-D-galactopyranosyl)-(1->4)-(methyl 2,3-di-O-benzoyl-β-D-glucopyranosyluronate)-(1->3)-2-deoxy-2-acetamido-β-D-galactopyranoside

Base Information

• Chemical Name: allyl (methyl 2,3-di-O-benzoyl-4-O-tert-butyldimethylsilyl-β-D-glucopyranosyluronate)-(1->3)-(2-deoxy-2-acetamido-β-D-galactopyranosyl)-(1->4)-(methyl 2,3-di-O-benzoyl-β-D-glucopyranosyluronate)-(1->3)-2-deoxy-2-acetamido-β-D-galactopyranoside
• CAS No.: 727991-30-2
• Molecular Formula: C₆₇H₈₂N₂O₂₇Si
• Molecular Weight: 1375.47

Synonyms:allyl (methyl 2,3-di-O-benzoyl-4-O-tert-butyldimethylsilyl-β-D-glucopyranosyluronate)-(1->3)-(2-deoxy-2-acetamido-β-D-galactopyranosyl)-(1->4)-(methyl 2,3-di-O-benzoyl-β-D-glucopyranosyluronate)-(1->3)-2-deoxy-2-acetamido-β-D-galactopyranoside

Chemical Property of allyl (methyl 2,3-di-O-benzoyl-4-O-tert-butyldimethylsilyl-β-D-glucopyranosyluronate)-(1->3)-(2-deoxy-2-acetamido-β-D-galactopyranosyl)-(1->4)-(methyl 2,3-di-O-benzoyl-β-D-glucopyranosyluronate)-(1->3)-2-deoxy-2-acetamido-β-D-galactopyranoside

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Technology Process of allyl (methyl 2,3-di-O-benzoyl-4-O-tert-butyldimethylsilyl-β-D-glucopyranosyluronate)-(1->3)-(2-deoxy-2-acetamido-β-D-galactopyranosyl)-(1->4)-(methyl 2,3-di-O-benzoyl-β-D-glucopyranosyluronate)-(1->3)-2-deoxy-2-acetamido-β-D-galactopyranoside

There total 1 articles about allyl (methyl 2,3-di-O-benzoyl-4-O-tert-butyldimethylsilyl-β-D-glucopyranosyluronate)-(1->3)-(2-deoxy-2-acetamido-β-D-galactopyranosyl)-(1->4)-(methyl 2,3-di-O-benzoyl-β-D-glucopyranosyluronate)-(1->3)-2-deoxy-2-acetamido-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

allyl (methyl 2,3-di-O-benzoyl-4-O-tert-butyldimethylsilyl-β-D-glucopyranosyluronate)-(1->3)-(4,6-O-p-methoxybenzylidene-2-deoxy-2-acetamido-β-D-galactopyranosyl)-(1->4)-(methyl 2,3-di-O-benzoyl-β-D-glucopyranosyluronate)-(1->3)-4,6-O-p-methoxybenzylidene-2-deoxy-2-acetamido-β-D-galactopyranoside → allyl (methyl 2,3-di-O-benzoyl-4-O-tert-butyldimethylsilyl-β-D-glucopyranosyluronate)-(1->3)-(2-deoxy-2-acetamido-β-D-galactopyranosyl)-(1->4)-(methyl 2,3-di-O-benzoyl-β-D-glucopyranosyluronate)-(1->3)-2-deoxy-2-acetamido-β-D-galactopyranoside (727991-30-2)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water; at 20 ℃; for 2h;

DOI:10.1021/ja0484045

Reference yield: 67.0%

allyl (methyl 2,3-di-O-benzoyl-4-O-tert-butyldimethylsilyl-β-D-glucopyranosyluronate)-(1->3)-(2-deoxy-2-acetamido-β-D-galactopyranosyl)-(1->4)-(methyl 2,3-di-O-benzoyl-β-D-glucopyranosyluronate)-(1->3)-2-deoxy-2-acetamido-β-D-galactopyranoside (727991-30-2) → allyl (methyl 2,3-di-O-benzoyl-4-O-tert-butyldimethylsilyl-β-D-glucopyranosyluronate)-(1->3)-(4,6-di-O-sodium sulfonato-2-deoxy-2-acetamido-β-D-galactopyranosyl)-(1->4)-(methyl 2,3-di-O-benzoyl-β-D-glucopyranosyluronate)-(1->3)-4,6-di-O-sodium sulfonato-2-deoxy-2-acetamido-β-D-galactopyranoside

Guidance literature:

With trimethyl-sulfo-ammonium betaine; In N,N-dimethyl-formamide; at 50 ℃; for 48h;

DOI:10.1021/ja0484045

Reference yield:

allyl (methyl 2,3-di-O-benzoyl-4-O-tert-butyldimethylsilyl-β-D-glucopyranosyluronate)-(1->3)-(2-deoxy-2-acetamido-β-D-galactopyranosyl)-(1->4)-(methyl 2,3-di-O-benzoyl-β-D-glucopyranosyluronate)-(1->3)-2-deoxy-2-acetamido-β-D-galactopyranoside (727991-30-2) → C61H68N2O27

Guidance literature:

With pyridine hydrogenfluoride; In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1021/ja0484045

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