8-[(4-methoxyphenyl)amino]pyrimido[5,4-d]pyrimidin-4(3H)-one O-benzyloxime

Base Information

• Chemical Name: 8-[(4-methoxyphenyl)amino]pyrimido[5,4-d]pyrimidin-4(3H)-one O-benzyloxime
• CAS No.: 1196086-82-4
• Molecular Formula: C₂₀H₁₈N₆O₂
• Molecular Weight: 374.402

Synonyms:8-[(4-methoxyphenyl)amino]pyrimido[5,4-d]pyrimidin-4(3H)-one O-benzyloxime

Chemical Property of 8-[(4-methoxyphenyl)amino]pyrimido[5,4-d]pyrimidin-4(3H)-one O-benzyloxime

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Technology Process of 8-[(4-methoxyphenyl)amino]pyrimido[5,4-d]pyrimidin-4(3H)-one O-benzyloxime

There total 3 articles about 8-[(4-methoxyphenyl)amino]pyrimido[5,4-d]pyrimidin-4(3H)-one O-benzyloxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

7-(benzyloxy)-8-imino-N-(4-methoxyphenyl)-7,8-dihydropyrimido[5,4-d]pyrimidin-4-amine (1196086-72-2) → 8-[(4-methoxyphenyl)amino]pyrimido[5,4-d]pyrimidin-4(3H)-one O-benzyloxime (1196086-82-4)

Guidance literature:

With hydrogenchloride; In ethanol; water; at 20 ℃; for 0.5h; chemospecific reaction; Reflux;

DOI:10.1002/ejoc.200900216

Reference yield:

7-(benzyloxy)-8-imino-N-(4-methoxyphenyl)-7,8-dihydropyrimido[5,4-d]pyrimidin-4-amine (1196086-72-2) → N-8-(4-methoxyphenyl)pyrimido[5,4-d]pyrimidine-4,8-diamine 3-oxide (1196086-81-3) + 8-[(4-methoxyphenyl)amino]pyrimido[5,4-d]pyrimidin-4(3H)-one O-benzyloxime (1196086-82-4)

Guidance literature:

With hydrogenchloride; In ethanol; water; at 20 ℃; for 0.833333h; Reflux;

DOI:10.1002/ejoc.200900216

Reference yield:

7-(benzyloxy)-8-imino-N-(4-methoxyphenyl)-7,8-dihydropyrimido[5,4-d]pyrimidin-4-amine (1196086-72-2) → N-8-(4-methoxyphenyl)pyrimido[5,4-d]pyrimidine-4,8-diamine 3-oxide (1196086-81-3) + 8-[(4-methoxyphenyl)amino]pyrimido[5,4-d]pyrimidin-4(3H)-one O-benzyloxime (1196086-82-4) + C20H18N6O2*ClH (1196086-88-0)

Guidance literature:

With hydrogenchloride; In ethanol; water; at 20 ℃; for 1.08333h; Reflux;

DOI:10.1002/ejoc.200900216

upstream raw materials:

7-(benzyloxy)-8-imino-N-(4-methoxyphenyl)-7,8-dihydropyrimido[5,4-d]pyrimidin-4-amine

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