trifluoromethanesulfonic acid 2-(2-oxo-2-phenylacetylamido)phenyl ester

Base Information

Chemical Name:trifluoromethanesulfonic acid 2-(2-oxo-2-phenylacetylamido)phenyl ester
CAS No.:1334682-12-0
Molecular Formula:C₁₅H₁₀F₃NO₅S
Molecular Weight:373.309
Hs Code.:

Synonyms:trifluoromethanesulfonic acid 2-(2-oxo-2-phenylacetylamido)phenyl ester

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Chemical Property of trifluoromethanesulfonic acid 2-(2-oxo-2-phenylacetylamido)phenyl ester

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Technology Process of trifluoromethanesulfonic acid 2-(2-oxo-2-phenylacetylamido)phenyl ester

There total 7 articles about trifluoromethanesulfonic acid 2-(2-oxo-2-phenylacetylamido)phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 1334683-40-7
C₁₄H₁₁NO₃

: 1334682-12-0
trifluoromethanesulfonic acid 2-(2-oxo-2-phenylacetylamido)phenyl ester

Guidance literature:: With pyridine; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol302119j DOI:10.1021/ol302119j

Reference yield:

: 611-73-4
Benzoylformic acid

: 1334682-12-0
trifluoromethanesulfonic acid 2-(2-oxo-2-phenylacetylamido)phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0 - 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

3: pyridine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

With pyridine; oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1021/ol302119j DOI:10.1021/ol302119j

Reference yield:

: 25726-04-9
phenylglyoxylyl chloride

: 1334682-12-0
trifluoromethanesulfonic acid 2-(2-oxo-2-phenylacetylamido)phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

2: pyridine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

With pyridine; triethylamine; In dichloromethane;
DOI:10.1021/ol302119j DOI:10.1021/ol302119j