1-<(N-benzyl-N-methylamino)methyl>-4,5-(methylenedioxy)phthalan hydrochloride

Base Information

Chemical Name:1-<(N-benzyl-N-methylamino)methyl>-4,5-(methylenedioxy)phthalan hydrochloride
CAS No.:104834-86-8
Molecular Formula:C₁₈H₁₉NO₃*ClH
Molecular Weight:333.815
Hs Code.:

Synonyms:1-<(N-benzyl-N-methylamino)methyl>-4,5-(methylenedioxy)phthalan hydrochloride

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Chemical Property of 1-<(N-benzyl-N-methylamino)methyl>-4,5-(methylenedioxy)phthalan hydrochloride

Chemical Property:

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Technology Process of 1-<(N-benzyl-N-methylamino)methyl>-4,5-(methylenedioxy)phthalan hydrochloride

There total 5 articles about 1-<(N-benzyl-N-methylamino)methyl>-4,5-(methylenedioxy)phthalan hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 104834-91-5
1-<(N-benzyl-N-methylamino)methyl>-4,5-(methylenedioxy)phthalide

: 104834-86-8
1-<(N-benzyl-N-methylamino)methyl>-4,5-(methylenedioxy)phthalan hydrochloride

Guidance literature:: With borane-THF; In tetrahydrofuran; for 8h; Heating;
DOI:10.1021/jm00384a030

Reference yield:

: 58343-48-9
5-formyl-benzo[1,3]dioxole-4-carboxylic acid

: 104834-86-8
1-<(N-benzyl-N-methylamino)methyl>-4,5-(methylenedioxy)phthalan hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: aq. KOH

2: 93 percent / H₂, conc. HCl / 20percent Pd/C / methanol; H₂O / 14 h / 50 °C / 2280 Torr

3: H₂ / Pd/C

4: H₂ / Pd/C

5: 46 percent / BH₃*THF / tetrahydrofuran / 8 h / Heating

With hydrogenchloride; potassium hydroxide; borane-THF; hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; water;
DOI:10.1021/jm00384a030

Reference yield:

: 104834-85-7
4,5-(methylenedioxy)-1-(nitromethyl)phthalide

: 104834-86-8
1-<(N-benzyl-N-methylamino)methyl>-4,5-(methylenedioxy)phthalan hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / H₂, conc. HCl / 20percent Pd/C / methanol; H₂O / 14 h / 50 °C / 2280 Torr

2: H₂ / Pd/C

3: H₂ / Pd/C

4: 46 percent / BH₃*THF / tetrahydrofuran / 8 h / Heating

With hydrogenchloride; borane-THF; hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; water;
DOI:10.1021/jm00384a030